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Lancaster <br /> Laboratories Analysis Report <br /> 5 New Holland Pike PO Box 12425 Lancaster PA 17605-2425+717-656 2300 Fax 717-6562681•www lancasterlabs com <br /> Page 2 of 9 <br /> Quality Control Summary <br /> Client Name ChevronTexaco Group Number 850017 <br /> Reported 05/11/03 at 11 26 PM <br /> Laboratory ComplIance Quality Control <br /> BlankBlank Report LCS LCSD LCS/LCSD <br /> Analysiq Name Result ML Units %REC $REC Limits &P 1) RPD Max <br /> Acenaphthene N D 1 u9/1 96 73-108 <br /> 2,4-Dinitrotoluene N D 1 ug/l 107 76-120 <br /> Fluorene N D 1 ug/l 91 65-115 <br /> 4-Chlorophenyl-phenylether N D 1 ug/1 97 68-108 <br /> Daethylphthalate N D 2 ug/l 89 70-108 <br /> N-Nitrosodiphenylamine N D 2 ug/l 89 67-106 <br /> 4-Bromophenyl-phenylether N D 1 ug/1 96 74-106 <br /> Hexachlorobenzene N D 1 ug/l 95 73-108 <br /> Phenanthrene N D 1 ug/l 99 72-106 <br /> Anthracene N D 1 ug/l 96 73-105 <br /> Di-n-butylphthalate N D 2 ug/l 92 75-107 <br /> Fluoranthene N D 1 ug/l 95 72-105 <br /> Pyrene N D 1 ug/l 98 71-111 <br /> Butylbenzylphthalate N D 2 ug/l 96 75-115 <br /> Benzo(a)anthracene N D 1 ug/l 102 75-107 <br /> Chrysene N D 1 ug/1 100 75-108 <br /> 3,31-Dichlorobenzidine N D 1 ug/l 85 30-108 <br /> bis(2-Ethylhexyl)phthalate N D 2 ug/3 101 72-117 <br /> D1-n-octylphthalate N D 2 ug/l 99 70-117 <br /> Benzo(b)fluoranthene N D 1 ug/l 102 74-110 <br /> Benzo(k)fluoranthene N D 1 ug/l 104 75-111 <br /> enzofa)pyrene N D 1 u9/1 104 79-110 <br /> enof1,2,3-cd)pyrene N D 1 ug/l 96 79-111 <br /> Wenz(a,h)anthracene N D 1 ug/l 105 84-117 <br /> e'.(g,h,i)perylene N D 1 ug/l 93 79-110 <br /> 2-Methylphenol N D 1 ug/1 67 62-98 <br /> 4-Methylphenol N D 2 u9/1 82 23-139 <br /> Benzyl alcohol N D 5 ug/1 81 54-100 <br /> Benzoic acid N D 6 ug/l 55 5-66 <br /> Batch number N031181AB Sample number(s) 4035278 <br /> Ethanol N D 50 ug/l 75 43-159 <br /> Methyl Tertiary Butyl Ether N D 0 5 ug/l 95 77-127 <br /> da-isopropyl ether N D 0 5 ug/l 91 74-125 <br /> Ethyl t-butyl ether N D 0 5 ug/l 82 74-120 <br /> t-Amyl methyl ether N D 0 5 ug/l 85 79-113 <br /> t-Butyl alcohol N D 5 ug/l 77 53-147 <br /> Dichlorodifluoromethane N D 2 u9/1 119 59-151 <br /> Chloromethane N D 1 ug/l 107 63-134 <br /> Vinyl Chloride N D 1 ug/l 112 71-129 <br /> Bromomethane N D 1 ug/l 94 42-126 <br /> Chloroethane N D 1 ug/1 112 54-127 <br /> Trichlorofluoromethane N D 2 ug/1 120 59-137 <br /> 1,1-Dichloroethene N D 0 8 ug/l 110 79-130 <br /> Methylene Chloride N D 2 ug/l 107 82-122 <br /> trans-1,2-Dichloroethene N D 0 8 ug/l 102 81-124 <br /> 1,1-Dichloroethane N D 1 ug/1 103 77-129 <br /> 2,2-Dichloropropane N D 1 ug/l 89 79-123 <br /> cis-1,2-Dichloroethene N D 0 8 ug/1 99 84-117 <br /> Chloroform N D 0 8 ug/l 100 86-124 <br /> Bromochloromethane N D 1 ug/l 106 58-136 <br /> 1,1,1-Trichloroethane N D 0 8 ug/l 95 83-127 <br /> Carbon Tetrachloride N D 1 ug/1 95 77-130 <br /> 1,1-Dichloropropene N D 1 u9/1 95 84-116 <br /> Benzene N D 0 5 ug/l 105 85-117 <br /> 1,2-Dichloroethane N D 0 5 ug/1 96 77-132 <br /> *-Outside of specification <br /> The result for one or both determinations was less than five times the LOQ <br /> } The background result was more than four times the spike added <br />