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W _Lancaster - <br /> Laboratories- <br /> Page 8 of 9 <br /> Quality Control Summary <br /> Client Name ChevronTexaco Group Number 839664 <br /> Reported 03/04/03 at 06 05 PM <br /> Surrogate Quality Control _ <br /> Hatch number 03031A53B <br /> TriflnnrnY_nlnPrtp-F <br /> 3986818 101 <br /> Blank 101 <br /> LCS 101 <br /> - MS - - -- 103 - - <br /> MSD 101 <br /> Limits 57-146 <br /> Analysis Name TCL SW846 Semivolatiles/Waters <br /> Batch number 03031WACO26 <br /> 2-Fluorophenol Phenol-d6 2,4,6-Tribromophenol Nitrobenzene-d5 <br /> 3986819 55 38 79 84 <br /> Blank 55 40 81 , B3 <br /> LCS 66 46 93 93 <br /> LCSD 65 45 93 94 <br /> Limits 22-96 10-87 36-147 45-139 • <br /> 2-Fluorobiphenyl Terphenyl-d14 <br /> 3986819 86 76 <br /> Blank 81 85 <br /> LCS ---9-5 93 <br /> LCS❑ _9 .`6 __ — -.----- - —_---90 <br /> -- Limits _— <br /> Analysis Name EPA SW846/8260 (water) - - - <br /> Batch number N030391AA <br /> Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene <br /> 3986819 99 ' 98 102 100 <br /> Blank 98 98 102 99 <br /> LCS 99 101 103 100 <br /> MS 99 101 102 100 <br /> MSD 100 100 101 99 <br /> Limits 86-118 80-120 r 88-110 86-115 <br /> Analysis Name BTEX + Oxygenates by 8260B <br /> Batch number P030382AA <br /> Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene <br /> 3986818 105 96 103 99 <br /> *- Outside of specification <br /> (1) The result for one or both determmatlons was less than five times the LOQ <br /> (2) The background result was more than four times the spike added .i <br /> Lancaster Laboratories Inc <br /> M E M e E 2425 New Holland Pike <br /> PO Box 12425 <br /> Lancaster PA 17605 2425 <br /> 717 656 2300 Fax 717-656 2681 111A wa 4A")In,) <br />