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Analysis • • <br /> Lancaster Laboratories <br /> • Where quality is a science <br /> Page 3 of 6 <br /> Lancaster Laboratories Sample No. WN 3930710 <br /> Collected 10/28/2002 11.51 by KK Account Number: 10906 <br /> Submitted. 10/31/2002 09 30 ChevronTexaco <br /> Reported- 11/13/2002 at 13.46 6001 Bollinger Canyon Rd L4310 <br /> Discard 12/14/2002 San Ramon CA 94583 <br /> MW-1-W-021028 Grab Water <br /> Facility# 98264 Job# 386854 GRD <br /> 3775 Tracy Blvd-Tracy T0607700627 MW-1 <br /> 264M1 <br /> As Received <br /> CAT As Received Method Dilution <br /> No Analysis Name CAS Number Result Detection units Factor <br /> Limit <br /> 03972 3,31-Dichlorobenzidine 91-94-1 N D 10 ug/1 1 <br /> 03973 bis(2-&thylhexyl)phthalate 117-81-7 N D 10 ug/l 1 <br /> 03974 Di-n-octylphthalate 117-84-0 N D 10 ug/l 1 <br /> 03975 Benzo(b)fluoranthene 205-99-2 N D 5 0 ug/l 1 <br /> 03976 Benzo(k)fluoranthene 207-08-9 N D 5 0 ug/l 1 <br /> 03977 Benzo(a)pyrene 50-32-8 N D 5 0 ug/l 1 <br /> 03978 rndeno(1,2,3-cd)pyrene 193-39-5 N D 10 ug/1 1 <br /> 03979 Dibenz(a,h)anthracene 53-70-3 N D 10 ug/l 1 <br /> 03980 Benzo(g,h,i)perylene 191-24-2 N D 5 0 ug/1 1 <br /> 04712 Benzyl alcohol 100-51-6 N D 5 0 ug/l 1 <br /> 04713 Benzoic acid 65-85-0 N D 10 ug/l 1 <br /> 05724 Misc Semivolatiles (Water) <br /> 00355 Aniline 62-53-3 N D 5 0 ug/l 1 <br /> Sufficient sample volume was not available to perform a MS/MSD for this <br /> analysis Therefore, a LCS/LCSD was performed to demonstrate precision and � <br /> accuracy at a batch level <br /> The recovery for aniline was outside ¢C limits in the LCS/LCSD associated <br /> with this sample The sample was re-extracted outside of the method <br /> required hold time on an extraction batch with compliant recovery for <br /> aniline in the LCS/LCSD Comparable sample results were observed between <br /> the two extractions The results reported are from the initial extraction <br /> of the sample <br /> 05382 EPA SW846/8260 (water) <br /> 05384 Dichlorodifluoromethane 75-71-8 N D 2 ug/l 1 <br /> 05385 Chloromethane 74-87-3 N D 2 ug/l 1 <br /> 05386 Vinyl Chloride 75-01-4 N D 1 ug/l 1 <br /> 05387 Sromomethane 74-83-9 N D 2 ug/1 1 <br /> 05388 Chloroethane 75-00-3 N D 2 ug/l 1 <br /> 05389 Trichlorofluoromethane 75-69-4 N D 2 ug/l 1 <br /> 05390 1,1-Dichloroethene 75-35-4 N D 1 ug/1 1 <br /> 05391 Methylene Chloride 75-09-2 N D 2 ug/l 1 <br /> 05392 trans-1,2-DYchloroethene 156-60-5 N D 1 ug/l 1 <br /> 05393 1,1-Dichloroethane 75-34-3 N D 1 u9/1 1 <br /> 05394 2,2-Dychloropropane 594-20-7 N D 1 ug/l 1 <br /> 5395 cis-1,2-Dichloroethene 156-59-2 N D 1 ug/l 3 <br /> 05396 Chloroform 67-66-3 N D 1 ug/1 1 <br /> ndanc�ster bortori s nc g <br /> #=Laborator detection limit <br /> N D=Not d aR@ spa it5orting Lima <br /> Lancaster PA 17b05 2425 <br /> 717 656 2300 Fax 717-65b 2681 2216 Rev 9111/00 <br />