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resolution capillary gas chromatography/mass spectroscopy <br /> (GC/MS) . PNAH compounds were mostly less than the detention <br /> Limits for each substance. Four organics were just over their <br /> limit for detection (Table 4) . <br /> The experimental sample yielded 80.6 milligrams of extractable <br /> hydrocarbon per gram of sample. The same four PNAH compounds <br /> were detected from the GC/MS analyses of this sample. In each <br /> case the concentration was less in the experimental than the <br /> control. This suggests that the source of PNAH compounds is from <br /> the asphalt and less from the fuel oil. All other volatile and <br /> semi--volatile orga>>ic compounds were below their respective <br /> detection limits (Table 4) . <br /> Heavy Metals Analyses <br /> The pavement samples were analyzed for both total and soluble <br /> heavy metals content pursuant to California hazardous waste <br /> regulations. Unlike the RCRA EP Toxicity criteria, the <br /> California Code of Regulations (CCR) , establishes limitations <br /> based upon both total content (i.e. , Total Threshold Limit <br /> Concentration; TTLC) and the extractable or soluble content <br /> (Soluble Threshold Limit Concentration; STLC . As one would <br /> expect, the established TTLC is always higher than the STLC. A <br /> waste is considered hazardous if the total concentration is equal <br /> to or greater than the TTLC, and non--hazardous if the total <br /> concentration is less than the STLC. However, if the total <br /> concentration for a given parameter is less than the TTLC but <br /> higher than or equal to the STLC, the sample is analyzed further <br /> - using the California Waste Extraction Test (WET) . If the <br /> concentration in the WET extract exceeds the STLC, the substance <br /> is deemed hazardous.4 <br /> The subject samples were digested and analyzed for total metals <br /> content by EPA Methods 3050 and 3010 as specified in CCR, Title <br /> 22, Section 66700 (b) . In both cases the heavy metals content was <br /> less than the TTLC and the STLC. 'Therefore, the WET was not <br /> performed. The sample results and the regulated concentration <br /> limits are summarized Table 5. These results indicate that the <br /> pavement samples would not be considered hazardous due to heavy <br /> metals content. <br /> Aquatic Bioassay <br /> Static aquatic bioassay tests were performed on both the <br /> experimental and control samples. The samples were milled to pass <br /> through a number 10 sieve and suspended in the test solution in <br /> accordance with procedures prescribed in Slandard.1fethods for the <br /> Examination tVater and iVastewater. Test mixtures containing 250 milligrams <br /> per liter (mg/1) and 750 mg/l of each sample were prepared fron <br /> tap--water-and__introduced-into--l0-liter-tanks.- Ten-fathead - --- <br /> minnows, Pimephales promelas, were placed into each tank <br /> approximately 20 minutes after the samples were introduced. <br />