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Spargero Analytical Laboratory DMslon <br /> Mobile Laboratory Division <br /> ry <br /> 41f&hnoloy lam, Scientific Dhrislon <br /> lith Automation in Mind <br /> EPA Method 6010/7471 <br /> Metals, CAM 17 <br /> MS 1 MSD Recoveries <br /> Attention Mr David Oliver Date Sampled Mar 12, 1999 <br /> ATC Associates, Inc Date Received Mar 12, 1999 <br /> P O Box 66 Date Analyzed Mar 18, 1999 Mercury <br /> Applegate, CA 95703 Mar 21, 1999 ICP <br /> Invoice# 10897MAR99 <br /> Project# 61059 0019 Project Name AT+T LODI <br /> Client ID MS/MSD LAB ID 10897-001A <br /> Matnx Sod Dilution 1 1 <br /> Units mg/kg <br /> Sample Spike MS % MSD % % <br /> Element Conc Conc MS Recovery MSD Recovery RSD <br /> Antimony (Sb) ND 500 232 464% 242 484% 42% <br /> Arsenic(As) ND 500 443 886% 471 942% 61% <br /> Barium(Ba) 107 500 131 480% 171 128% 91% <br /> Beryllium (Be) 0 336 100 858 824% 929 895% 83% <br /> Cadmium (Cd) 1 11 200 162 755% 176 825% 89% <br /> Chromium (Cr) 301 500 613 624% 754 906% 37% <br /> Cobalt(Co) 729 200 222 746% 274 101% 30% <br /> Copper(Cu) 205 500 617 824% 71 5 102% 21% <br /> Lead (Pb) 217 500 418 793% 460 877% 10% <br /> Mercury (Hg) ND 00500 00568 114% 00623 1246% 92% <br /> Molybdenum (Mo) ND 500 418 836% 464 928% 10% <br /> Nickel (Ni) 197 100 103 833% 119 993% 18% <br /> Selenium (Se) ND 500 382 764% 392 784% 26% <br /> Silver(Ag) ND 500 304 608% 284 568% 68% <br /> Thallium (TI) ND 500 403 806% 420 840% 41% <br /> Vanadium (V) 592 200 765 865% 834 121% 33% <br /> Zinc (Zn) 441 500 810 738% 937 992% 29% <br /> ppm=parts per million-mg/kg=milligram per kilogram <br /> ND=Not Detected Compound(s)may be present at concentrations below the detection Irma <br /> Note If sample concentration is higher than spike concentration,recoveries may be either high or low <br /> Note If sample concentration Is lower than spike concentraUon recoveries may be either high or low due to matrix interference <br /> /11,1,1� Mar 21, 1999 <br /> E McKinney, Inorganics Manager Date Reported <br /> SPARGER TECHNOLOGY ANALYTICAL LABORATORY INC IS CERTIFIED BY THE STATE OF CALIFORNIA <br /> DEPARTMENT OF HEALTH SERVICES AS A HAZARDOUS WASTE TESTING LABORATORY <br /> iCertdication No 16141 <br /> CAM17MSS As <br /> 30,50 Fite Crcle Suite 112 • Sacramento California 95827 • (996) 362-8947 9 FAX(996) 362-0947 <br />