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' Alpha Analytical, Inc. <br /> 255 Glendale Ave • Suite 21 • Sparks,Nevada 89431-5778 <br /> 4A (775)355-1044 • (775)355-0406 FAX• 1-800-283-1183 <br /> ate Work Order <br /> '*�Jqn-04� QC Summary Report <br /> 03121947 <br /> ' Method Blank Type MBLK Test Code EPA Method SW8260B <br /> File ID D\MSDCHEM1MS121DATA1031224103122407 D Batch ID MS12W1224A Analysts Date 12/24/2003 11 55 <br /> Sample ID MBLK MS12W1224A Units kg/L Run ID GC/MSD_12 031224A Prep Date 12/24/2003 <br /> ' Analyte Result PQL SpkVal SpkRefVal %REC LowUmit HighLimit RPDRefVal %RPD(Limit) Qual <br /> Benzene ND 05 <br /> Toluene ND 05 <br /> othvlbenzene ND 05 <br /> p-Xylene ND 05 <br /> -Xylene ND 05 <br />' Laboratory Control Spike Type LCS Test Code EPA Method SW8260B <br /> File ID D 1MSDCHEM1MS121DATA1031224\03122408 D Batch ID MS12W1224A Analysts Date 12/24/2003 12 17 <br /> Sample ID LCS MS12WI224A Units pg/L Run ID GC/MSD_12_031224A Prep Date 12/24/2003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowUmd HighLimit RPDRefVal %RPD(Limit) Qual <br />' Benzene 102 05 10 102 83 119 <br /> Toluene 991 05 10 99 80 120 <br /> Ethvlbenzene 101 0 5 10 101 so 120 <br /> m,p-Xylene 22 05 20 110 77 125 <br /> o-Xylene 104 05 10 104 77 124 <br /> Sample Matrix Spike Type MS Test Code EPA Method SW8260B <br /> File ID D 1MSDCHEM1MS121DATA1031224103122411 D Batch ID MS12W1224A Analysis Date 12/24/2003 13 25 <br />' Sample ID 03121921-01 AMS Units pg/L Run ID GC/MSD_12_031224A Prep Date 12/24/2003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLtmit HighUmit RPDRefVal %RPD(Limit) Qual <br /> Benzene 511 1 3 50 0 102 59 145 <br /> Toluene 495 1 3 50 0 99 39 161 <br /> ylbenzene 51 1 3 50 0 56 101 57 145 <br /> IW-Xylene 111 13 100 0 111 37 163 <br /> o-XVlene 52 2 1 3 50 0 104 47 156 <br />' Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW8260B <br /> File ID D 1MSDCHEMIMS121DATA1031224103122412 D Batch ID MS12W1224A Analysis Date 12/24/2003 13 47 <br /> Sample ID 03121921-01AMSD Units pg/L Run ID GC/MSD-12-031224A Prep Date 12/24/2003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPDRefVal %RPD(Limit) Qual <br /> Benzene 503 1 3 50 0 101 59 145 51 13 1 6(22) <br /> Toluene 49 1 3 50 0 98 39 161 4945 0 9(22) <br /> Ethvlbenzene 509 1 3 50 056 101 57 145 5096 0 1(22) <br /> m p-Xylene 109 1 3 100 0 109 37 163 1109 1 8(23) <br />' o-XVlene 51 8 1 3 50 0 104 47 156 5224 0 8(50) <br /> Comments <br /> Calculations are based off of raw(non-rounded)data However,for reporting purposes,all QC data is rounded to three significant figures Therefore,hand calculated <br /> values may differ slightly <br /> �'0 <br />