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QC Report Matrix Spike/Matrix Spike Duplicate Report Number 29930 Date 12/3!2002 Protect Name ARC Pump $ Weld Project Number Duplicate Spiced Spikied to Spiked ame e Relative Spiked Sample Spike Dupe Samp a Same a Sample Sample Relative Percent Percent Parameter Sample Value Level Level Value Value Units Methods Ante alyzed Recov t Recov t Percent Re�clov Droit Benzene 29974-01 <0 50 402 38 2 41 0 Toluene 29974-01 <0 50 402 38 2 426 40 6 ug/L EPA 82606 11/ug/L EPA 8260B 26/02 106 16/02 102 05 0 53 70-130 25 70-130 25 Tert-Butanol 29974-01 76 201 191 200 204 ug/L EPA 8260B 11/26/02 959 102 6 753 70-130 25 Methyl-t-Butyl Ether 29974-01 10 402 382 56 4 579 ug/L EPA 8260B 11/26/02 115 125 816 70-130 25 Benzene 29980-01 11 400 400 55 3 515 ug/L EPA 8260B 11/24/02 111 101 897 70-130 25 Toluene 29980-01 6 5 400 400 50 0 459 ug/L EPA 82606 11/24/02 109 985 100 70-130 25 Tert-Butanol 29980-01 <5 0 200 200 216 197 uglL EPA 82606 11/24/02 108 983 950 70-130 25 Methyl-t-Butyl Ether 29980-01 <0 50 400 400 443 41 6 ug/L EPA 8260B 11/24/02 111 104 638 70-130 25 Benzene 30059-01 <0 50 400 400 422 Toluene 40 6 ug/L EPA 82608 11/27/02 106 101 401 70-130 25 30059-01 <0 50 400 400 423 404 ug/L EPA 8260E 11/27/02 106 101 445 70-130 25 Tert-Butanol 30059-01 78 200 200 213 207 ug/L EPA 82606 11/27/02 103 998 301 70-130 25 Methyl-t-Butyi Ether 30059-01 450 400 400 498 494 ug/L EPA 82606 11/27/02 124 116 683 70-130 25 I Benzene 30055-02 <0 50 400 400 392 373 ug/L EPA 8260B 11/30/02 981 932 510 70-130 25 Toluene 30055-02 <0 50 400 400 368 34 9 ug/L EPA 8260B 11/30/02 92 1 872 544 70-130 25 Tert-Butanol 30055-02 <5 0 200 200 202 210 ug/L EPA 82606 11/30/02 101 Methyl-t-Butyl Ether 30055-02 <0 50 400 105 356 70-130 25 40 0 36 8 36 1 uglL EPA 8260B 11/30/02 919 902 181 70-130 25 KIFF ANALYTICAL, LLC Approved By Joel Kill 2795 2nd 5t, Suite 300 Davis, CA 95616 530-297-4800 V