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MINIMUM V <br /> ERIFICA'IION LABORAIORY ANALYSIS <br /> TANK TANK Mi-O "ITH-D BZ X & E CL l IC TOTAL EDB METALS Pt-B <br /> * CONTENTS 8015 8015 8020 8010 LEAD ICAPI 8270 <br /> 8260 8260 8260 8240 7420 8240 AES or <br /> 7421 AA <br /> LEADED .tt�, x X X <br /> 464 OAS 3C <br /> UNL OAS X X <br /> DIESEL X X <br /> KEROSENE X X <br /> UNK FUEL X X X X X <br /> OIL X X <br /> CI II.OR <br /> SOLVENTS X X <br /> i NONCIILOR <br /> SOLVENTS X <br /> WASTIA <br /> USED 011, x LX I x x x <br /> All analyses methods are designated EPA methods described In EPA SW 846,Third Edition Those methods not found In <br /> SW 846,are specifically noted below Refer to the"SWRCH LUF'F Field Manual% Appendix A-20,Table 3-5 for deleLiion <br /> limits of motor vehicle fuels (gasoline and diesel) Refer to 1-2-3 "Regional Board Staff Recommendations for luilfal <br /> Evaluation and Investigation of US 1'3" for the waste and motor oil detection limits <br /> Detecilon Llmlls that remain below the MCI, 811.0 or Allowable I butt of Zile c011ilUnhhlhhlt III question will be accel)'", <br /> however laboratory shall usllize Tile most conservative method <br /> 1 ABORAIbRY ANALYSES TERMINOLOGY: <br /> 7 PI I-0 'Total petroleum I lydrocaibon, Gasoline, OC/FID {5030) 8015 mod or GCJINS 8260 <br /> '11311-D 'total petroleum Ilydrocaibon, Diesel, OC/FID (3550), 8015 mod or ODMS 8260 <br /> B i'X & E Benzene, Toluene, Xylene & Ethyl Benzene, OC/PID 8020 or OC/MS 8260 <br /> CL 11C Chlorinated llydrocarbon, oC/IISD 8010, OC/MS 8240 <br /> Total Lead Total lead, AA 7420, AA 7421 or ICP-AES 6010 <br /> EDB Ethylene dibrotnide (DIIS-A8 1803), OC/MS 8240 (DIIS-Luft) <br /> OC FID (las Chrainatography, Flame Ionizalson Delectlon <br /> ICAP or AA Inductively Coupled Plasma Atomic Emission Spectrometry 61110 or Atomic Absorption <br /> Spectrometry 70X10 Metals: Cadmium, Chromium III and V1, lead, slid Zine. <br /> PCB Polychlorinaled 111phenyls, ODMS 8270 or 8080 <br /> Method 3050 Acid digestion <br /> Method 3540 Soxhlet sample preparation <br /> Method 3550 Sonication sample preparation, extraction method <br /> Method 5030 Purge and trap sample preparalion <br /> QA/QC Quailly Assurance/Quality Control <br /> Notes: To avoid false positive detection of benrene, benzene free solvents are to be used Fused capillary colurnus are <br /> . preferred to packed columns', a packed column may be used as a "first cut" with "dlrly" samples or once the hydiotatboas <br /> have been characterized and proper QA/AC Is followed <br /> For Drinking water sources, EPA recommends that the 500 series for volatile organics be used in preference to the 600 sc.i its <br /> because the delecilob limits are lower the QA/QC is better. <br /> Ell 23 048 (Rev I In190) I} <br /> i <br />