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II <br /> SIE <br /> k <br /> BTEX MATRIX SPIKE REPORT <br /> EPA METHOD 5030 WITH, GC/PTD <br /> ANAMETRIX, INC. (408)! 432-8192 <br /> Sample T.D. : 2-91-441-ST 4 Anametrix I.D. : 9103121-04 <br /> MatrDateiS0IL Analyst <br /> ampled a 03/07/91 . <br /> Supervisor : <br /> Date Analyzed / /zed 03 14 91 03 <br /> Date Released 03/21/91 � <br /> SPIKE REC REC &REC <br /> COMPOUND AMT. MS MS MSD MSD RPA LIMITS <br /> (m5/K5) (mg/Kg) K ,� <br /> -------------^---------___ .__--------- m --------------------------- - <br /> Benzene 0. 010 0. 009 94% 0.011i` 106% 12& 49-159 <br /> Toluene 0. 010 0.010 96-% 0.011 1081% 12% 53-156 <br /> Ethylbenzene 0. 010 0.010 96%' 0. 011 1141 15%. 54-151 <br /> M+P-Xylenes 0.0067 0.0065 96% 0. 008 ! 114% 17% 56-157 <br /> O-Xylene 0.0033 0.0032 95% 0.004 i 110% 14% 58-154 <br /> -------------------------------------- ^_-__- -------^^-^^--W--- <br /> i I <br /> it <br /> i <br /> jrf <br /> f <br /> i <br /> r f <br /> i ffff <br /> II <br /> _f _ <br /> QUALITY ASSURANCE .� TPH PAGE 1 <br /> i4 Y <br /> ., n <br />