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110 2nd Avenue Souta,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> .4 http://www.mccampbell.com E-mail:main@mccampbell.com <br /> Advanced GeoEnvironmental Client Project ID: Robert Metals Date Sampled: 02/08/01 <br /> 837 Shaw Road Date Received:02/13/01 <br /> Stockton,CA 95215 Client Contact: Paul Dotson Date Extracted:02/13/01 <br /> [Client P.O: Date Analyzed:02/13/01 <br /> Volatile Halocarbons <br /> EPA method 601 or 8010 <br /> Lab ID 59985 59987 59990 59993 <br /> Client ID P1-5 P2-5 P3-5 P4-5 <br /> Matrix S S S S <br /> Compound Concentration <br /> Bromodichloromethane ND ND ND ND <br /> Bromoform ND ND ND ND <br /> Bromomethane ND ND ND ND <br /> Carbon Tetrachloride(c) ND ND ND ND <br /> Chlorobenzene ND ND ND ND <br /> Chloroethane ND ND ND ND <br /> 2-Chloroethyl Vinyl Ether ND ND ND ND <br /> Chloroform` ND ND ND ND <br /> Chloromethane ND ND ND ND <br /> Dibromochloromethane ND ND ND ND <br /> 1,2-Dichlorobenzene ND ND ND ND <br /> 1,3-Dichlorobenzene ND ND ND ND <br /> 1,4-Dichlorobenzene ND ND ND ND <br /> Dichlorodifluoromethane ND ND ND ND <br /> 1,1-Dichloroethane ND ND ND ND <br /> 1,2-Dichloroethane ND ND ND ND <br /> 1,1-Dichloroethene ND ND ND ND <br /> cis 1,2-Dichloroethene ND ND ND ND <br /> trans 1,2-Dichloroethene ND ND ND ND <br /> 1,2-Dichloropropane ND ND ND ND <br /> cis 1,3-Dichloropropene ND ND ND ND <br /> trans 1,3-Dichloropropene ND ND ND ND <br /> Methylene Chloride(l) ND<25 ND<25 ND<25 ND<25 <br /> 1,1,2,2-Tetrachloroethane ND ND ND ND <br /> Tetrachloroethene ND<15 ND<15 ND<15 ND<15 <br /> 1,1,1-Trichloroethane ND ND ND ND <br /> 1,1,2-Trichloroethane ND ND ND ND <br /> Trichloroethene ND ND ND ND <br /> Trichlorofluoromethane ND ND ND ND <br /> Vinyl Chlorides ND ND ND ND <br /> %Recovery Surrogate 94 94 92 94 <br /> Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in ug/L,soil and sludge samples in ug/kg, wipe samples in ug/wipe <br /> Reporting limit unless otherwise stated:water/TCLP/SPLP extracts,ND<0.5ug/L;soils and sludges,ND<5ug/kg;wipes,ND<0.2ug/wipe <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (b)tribromomethane;(c)tetrachloromethane;(d)(2-chloroethoxy)ethene;(e)trichloromethane;(f)dichloromethane;(g)chloroethene;(h)a <br /> lighter than water immiscible sheen is present;(i)liquid sample that contains greater than—5 vol.%sediment;0)sample diluted due to high <br /> organic content. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />