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Report Number: 68735 QC Report: Matrix Spike/Matrix Spike Duplicate Date: 06/08/2009 Project Name: Former American Forest Products Project Number: 17322736 Duplicate Spiked Duplicate Spiked Spiked Sample Relative Spike Spiked Spiked Sample Sample Relative Percent Percent Spiked Sample Spike Dup. Sample Sample Analysis Date Percent Percent Percent Recov. Diff. Parameter Sample Value Level Level Value Value Units Method Analyzed Recov. Recov. Diff. Limit Limit TPW-D (Si Gel) BLANK <50 1000 1000 837 894 ug/L M EPA 8015 614109 83.7 89.4 6.63 70-130 25 1,1-Dichloroethane 68724-06 <0.50 40.3 40.3 42.8 42.7 uglL EPA 8260B 6/4109 106 106 0.274 70-130 25 1,2-Dichloroethane 68724-06 <0.50 40.8 40.8 41.8 42.0 ug/L EPA 82606 614109 103 103 0.344 70-130 25 Benzene 6872406 <0.50 40.6 40.6 41.9 41.4 ug/L EPA 8260B 614109 103 102 1.11 70-130 25 Chlorobenzene 68724-06 <0.50 40.1 40.1 39.2 39.1 ug/L EPA 82606 614109 97.8 97.5 0.322 70-130 25 Methyl-t-butyl ether 68724-06 1.1 40.7 40.7 41.8 41.8 ug/L EPA 8260B 614109 100 100 0.106 70-130 25 j Tert-Butanol 68724-06 <5.0 201 201 206 206 ug/L EPA 82608 614109 102 102 0.142 70-130 25 Toluene 68724-06 <0.50 40.1 40.1 41.2 40.7 ug/L EPA 8260E 614109 103 102 1.21 70-130 25 1;1=Dichloroethane 68733-01 <(Y5OF--40.3 4(Y3 42.0 4'i 1 ug/L--E-PA-82606 6I51091C4---f02 214 70=130-5 1,2-Dichloroethane 68733-01 <0.50 40.8 40.8 41.6 40.5 ug/L EPA 8260B 615/09 102 99.5 2.48 70-130 25 Benzene 68733-01 68 40.6 40.6 108 105 ug/L EPA 8260B 615/09 97.4 90.7 7.13 70-130 25 Chlorobenzene 68733-01 <0.50 40.1 40.1 39.0 38.3 ug/L EPA 8260B 615/09 97.4 95.6 1.84 70-130 25 Methyl-t-butyl ether 68733-01 <0.50 40.7 40.7 39.8 39.6 ug/L EPA 82606 615/09 97.7 97.1 0.588 70-130 25 Tert-Butanol 68733-01 9.5 201 201 219 218 ug/L EPA 8260B 6/5/09 104 104 0.226 70-130 25 Toluene 68733-01 2.5 40.1 40.1 42.8 41.6 ug/L EPA 82606 615109 101 97.6 3.11 70-130 25 KIFF ANALYTICAL, LLC 2795 2nd Street, Suite 300 Davis, CA 95618 530-297-4800