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D&N laboratories QUALITY CONTROL REPORT Reported: 24-MAY-95 x`S SH+Y}^i. f4� +tK.;.u.'i f}`.`vIL6 ^ G N4 xvA].ry °>v.,: ��f�,'=,��i ✓�1�.�.-��+�'GY tE� } >•Q{w.k..'£n�n^J.�iit�a'�:w"`Ci J,vA2:.�r� w. AIXTs+...v}?I$:'i Lab Id WG7448-2 Sample Id: Matrix Spike Parameter - Vatue Units Spike Units A Ree v Extramd AltalyzedE 4-Chloro-3-Methylphenol 3.50 mg/Kg 3.75 mg/Kg 93.% 24-APR-95 25-APR-95 2-Chlorophenol 3.27 mg/Kg 3.75 mg/Kg 87.% 24-APR-95 25-APR-95 4-Nitraphenol 2.64 mg/Kg 3.75 mg/Kg 70.% 24-APR-95 25-APR-95 Pentachtorophenot 3.43 mg/Kg 3.75 mg/Kg 92.% 24-APR-95 25-APR-95 Phenol 3.05 m9/K9 3.75 mg/Kg 81.% 24-APR-95 25-APR-95 Acenaphthene 2.49 mg/Kg 2.5 mg/Kg 100% 24-APR-95 25-APR-95 1,4-dichlorobenzene 2.23 mg/Kg 2.5 mg/Kg 89.% 24-APR-95 25-APR-95 2,4-Dinitrototuene 2.20 mg/K9 2.5 mg/Kg WA 24-APR-95 25-APR-95 N-Nitroso-di-n-Propylamine 2.27 mg/Kg 2.5 mg/Kg 91.% 24-APR-95 25-APR-95 Pyrene 2.48 mg/Kg 2.5 mg/Kg 99.% 24-APR-95 25-APR-95 1,2,4-Trichlorobenzene 2.45 mg/KO 2.5 mg/Kg 98.% 24-APR-95 25-APR-95 Surrogate: 2-Ftuorophenot 75.1 % 24-APR-95 25-APR-95 Phenot-dS 86.0 % 24-APR-95 25-APR-95 Nitrobenzene-d5 82.8 % 24-APR-95 25-APR-95 2-Ftuorobiphenyl 90.4 % 24-APR-95 25-APR-95 2,4,6-Tribromophenot 83.5 % 24-APR-95 25-APR-95 Terphenyl-dl4 86.6 % 24-APR-95 25-APR-95 2-Chtorophenot-d4 92.1 % 24-APR-95 25-APR-95 1,2-Dichtorobenzene-d4 67. % 24-APR-95 25-APR-95 Lab Id: WG7448-3 Sample Id: Matrix Spike Dup Parameter Vatue Units X lte .RPD Utracted Analyzed 4-Chloro-3-Methytphenot 3.36 mg/Kg 90.% 3.5 24-APR-95 25-APR-95 2-Chtorophenol 3.25 mg/Kg 87.% 0.61 24-APR-95 25-APR-95 4-Nitrophenot 2.63 mg/Kg 70.% 0.38 24-APR-95 25-APR-95 Pentachlorophenol 3.43 mg/Kg 92.X 0.0 24-APR-95 25-APR-95 Phenol 2.99 mg/Kg 80.% 2.0 24-APR-95 25-APR-95 Acenaphthene 2.50 mg/Kg 100% 0.40 24-APR-95 25-APR-95 1,4-dichlorobenzene 2.16 mg/Kg 86.% 3.2 24-APR-95 25-APR-95 2,4-Dinitrotoluene 2.21 mg/Kg 88.X 0.45 24-APR-95 25-APR-95 N-Nitroso-di-n-PropyLamine 2.26 mg/Kg 90.% 0.44 24-APR-95 25-APR-95 Pyrene 2.46 mg/Kg 98.% 0.81 24-APR-95 25-APR-95 1,2,4-Trichtorobenzene 2.42 mg/Kg 97.% 1.2 24-APR-95 25-APR-95 Surrogate: 2-Ftuorophenol 74.9 X 24-APR-95 25-APR-95 Phenol-d5 85.5 % 24-APR-95 25-APR-95 Nitrobenzene-d5 83.5 % 24-APR-95 25-APR-95 2-Fluorobiphenyt 91.2 % 24-APR-95 25-APR-95 2,4,6-Tribromophenol 82.9 % 24-APR-95 25-APR-95 Terphenyt-d14 87.5 % 24-APR-95 25-APR-95 2-Chtorephenot-d4 91.0 % 24-APR-95 25-APR-95 1,2-Dichlorobenzene-d4 66.2 % 24-APR-95 25-APR-95