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t <br /> ** SPL BATCH QUALITY CONTROL REPORT ** HOUSTON LABORATORY <br /> State of Tennessee Method for Diesel 8880 INTERCHANGE DRIVE <br /> 0 HOUSTON, TEXAS 77054 <br /> PHONE(713)660-0901 <br /> Matrix: Aqueous Batch Id: HPTT971031021300 <br /> ' Units: mg/L <br /> L A B O R A T O R Y C O N T R O L S A M P L E <br /> 1 S P I K E Method Spike Blank Spike QC Limits(**) <br /> C 0 M P 0 U N D S Blank Result Added Result Recovery (Mandatory) <br /> <2> <3> <1> k I Recovery Range <br /> ' Diesel ND 5.0 4.3 86.0 53 - 148 <br /> ' M A T R I X S P I K E S <br /> S P I K E Sample Spike Matrix Spike Matrix Spike MS/MSD QC Limits(***) <br /> C O M P O U N D S Results Added Duplicate Relative t (Advisory) <br />' Result Recovery Result Recovery Difference RPD <br /> <2> <3> <1> <4> <1> <5> Max. Recovery Range <br /> tDIESEL 0.72 5.0 3.9 63.6 4.5 75.6 17.2 39 21 - 175 <br /> Analyst: APR = values Outside OC Range. = Data outside Method Specification limits. <br /> Sequence Date: 10/31/97 NC = Not Calculated (Sample exceeds spike by factor of 4 or more) <br /> SPL ID of sample spiked: 971OA45-06B ND = Not Detected/Below Detection Limit <br /> Sample File ID: TTJ4058.TX0 t Recovery = [( <1> - <2> ) / <3> ] x 100 <br /> Method Blank File ID: LCS 1: Recovery = (<l> / <3> ) x 100 <br /> Blank Spike File ID: TTJ4119.TX0 Relative Percent Difference = 1 (<4>' - <5> I / [(e4> + <5> ) x 0.51 x 100 <br /> Matrix Spike File ID: TTJ4059.TX0 (**I = Source: SPL Historical Limits 1st Qtr'97 and 4th Qtr'97 <br /> Matrix Spike Duplicate File ID: TTJ4060.TX0 (***) Source: SPL Historical Limits 1st Qtr. '97 and 4th Qtr.197 <br />' SAMPLES IN RATCH(SPL IDJ_ 971OA45-07B 9710AD1-01B 971OA01-02B 9710A01-032 <br /> 971OA01-0413 971OA01-05B 971OA45-106 971OA45-06B <br /> 971DA45-08B 971OA45-09B <br /> i <br /> 1 <br /> 1 - . <br />