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Alpha Analytical, Inc. <br /> 255 Glendale Ave. • Suite 21 • Sparks,Nevada 89431-5778 <br /> ' (775)355-1044•(775)355-0406 FAX• 1-800-283-1183 <br /> Date: e Work Order: <br /> 24-Sep-14 QC Summary Report 14091701 <br /> ethod Blank Type MBLK Test Code: EPA Method SW8015B/C/SW8260B <br /> Ile ID: 14092304.13 Batch ID: MSISW0923B Analysis Date: 09/23/201411:09 <br /> Sample ID: MBLK MS15W0923B Units: mg/L Run ID:MSD_15_140923A Prep Date: 09/23/201411:09 <br /> nalyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDRefVal %RPD(Limit) Qual <br /> PH-P(GRO) ND 0.5 <br /> Surr: 1,2-Dichloroethane-d4 0.00971 0.01 97 70 130 <br /> Surr:Toluene-d8 0.00979 0.01 98 70 130 <br /> urr:4-Bromofluorobenzene 0.0115 0.01 115 70 130 <br /> Ikaboratory Control Spike Type LCS Test Code: EPA Method SW8015B/C/SW8260B <br /> File ID: 14092303.D Batch ID:MSISW0923B Analysis Date: 09/23/201410:35 <br /> ample ID: GLCS MS15W0923b Units: mg/L Run ID:MSD_15_140923A Prep Date: 09123/201410:35 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDRefVal %RPD(Limit) Qual <br /> TPH-P(GRO) 0.346 0.05 0.4 86 70 130 <br /> Surr: 1,2-Dichloroethane-d4 0.0098 0.01 98 70 130 <br /> turr:Toluene-d8 0.00973 0.01 97 70 130 <br /> urr:4-Bromofluo robe nzene 0.0117 0.01 117 70 130 <br /> Sample Matrix Spike Type MS Test Code: EPA Method SW8015B/C/SW8260B <br /> File ID: 14092310.13 Batch ID:MS15W0923B Analysis Date: 09/231201413:33 <br /> ample ID: 14091143-01 AGS Units: mg/L Run ID:MSD_15_140923A Prep Date: 09/23/2014 13:33 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDRefVal %RPD(Limit) Qual <br /> tTsurPH-P(GRO) 1.85 0.25 2 0 93 54 143 <br /> urr: 1,2-Dichloroethane-d4 0.0537 0.05 107 70 130 <br /> r: <br /> Toluene-d8 0.0469 0.05 94 70 130 <br /> Surr:4-Bromofluorobenzene 0.056 0.05 112 70 130 <br /> ample Matrix Spike Duplicate Type MSD Test Code: EPA Method SW8015B/C I SW8260B <br /> File ID: 14092311.13 Batch ID:MS16W0923B Analysis Date: 09/23/2014 13:56 <br /> Sample ID: 14091143-01AGSD Units: mg/L Run ID:MSD_15_140923A Prep Date: 09/23/201413:56 <br /> .Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDRefVal %RPD(Limit) Qual <br /> TPN-P(GRO) 1.85 0.25 2 0 93 54 143 1.85 0.2(23) <br /> Surr: 1,2-Dichloroethane-d4 0.0556 0.05 111 70 130 <br /> Surr:Toluene-d8 0.0469 0.05 94 70 130 <br /> Surr:4-Bromofluo robe nzene 0.0549 0.05 110 70 130 <br /> Comments: <br /> Calculations are based off of raw(non-rounded)data.However,for reporting purposes,all QC data is rounded to three significant figures.Therefore,hand calculated <br /> (values may differ slightly. <br /> i <br /> t <br /> 1 <br /> t <br />