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• • Enviro-Chem, Inc. 1214 E. Lexin ton Avenue, Poona, CA 91766•Tel (909)5 -590 (949)5W5j07 8270C QA/QC Report Matrix:— Soil/Solid/Sludge/Oil it: /K PPM • Date Analyzed: 7/19/2018 � S (%S)/M*4 Spik&Rplicate (MSD)• L'db I.D.. 0180719-LCS1/2 Analyte SR spk conc MS %MS MSD %MSD %R—PD- ACP %MS ACP RPD Phenol 0.0 2.00 1.97 98% 1.91 96% 3% 50-150 0-20 PyreneO 100.0012.00 1 2.06 W 1 103%01 2.02 10101%01 2% 1 50-150 1 0-20 Laboratory Control Spike (LCS): Analyteg spk conc I LCS % RC ACP%RC • Phenol 2.00 2.03 101% 75-125 • 1,4-Dichlorobenzene 2.00 2.02 101% 75-125 , 2,4-Dichloro henol 2.00 2.06 103% 75-125 Hexachlorobutadiene 0 2.00 2.05 102% 75-125 • 4-Chloro-3-meth I henol 1 2.00 1 2.00 1 100% 75-125 , Fluoranthene 1 2.00 1 1.70 85% 75-125 • • • • • 1--- Surrogate Recovery spk conc I ACP% °oRC I %RC %RC I %RC I %RC %RC I %RC Sample I.D. MB 180718-24 2-Fluorophenol 40 25-121 88% 101% Phenol-d5 40 24-113 2% 90% Nitrobenzene-d5 40 23-120 8 % 90% 2-Fluorobi hen I 40 30-115 96 0 103% 2,4,6-Tribromo henol 40 19-122 680 72% Ter hen I-d14 400, 18-137 118% 1120/691 Surrogate Recovery spk conc ACP% %RC %RC %RC %RC %RC %RC I W%RC • Sample I.D. 10 0 • 2-Fluorophenol 40 25-121 Phenol-d5 40 24-113 Nitrobenzene-d5 40 23-120 2-Fluorobi hen I 40 30-115 2,4,6-Tribromo henol 40 19-122 • Terphenyl-dl4o 1 4001 18 61 • Surrogate Recovery I spk conc I ACP% I %RC %RC I %RC 1 %RC 491 %RC I %RC I*%RC Sample 1.D- - -2-Fluorophenol 40 25-121 Phenol-d5 40 24-113 • Nitrobenzene-d5 40 23-120 2-Fluorobi hen I 40 30-115 • 2,4,6-Tribromo henol 1 40 01 19-122 1 el Ter hen I-d14 40 18-137 Surrogate fail due to matrix interference • • • e: LCS,�S, WD a(S iWoOWNore resu is ar in con ro, Analyzed and Reviewed By. F'na eviewer"