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Mai 16 2006 12:20PM U�First Loc.370 <br />(2Q9)941-4022 <br />05/16/2006 09:57 707-745-6297 PSC <br />Mey 16 2006 10:47RM McCAMPBELL ANALYTICAL 9PS798461P <br />QC SUMMARY REPORT FOR SW8270D <br />W.O. Semple Mebla Sall OG M9trix: Sail <br />P.8 <br />PA( iE 08112 <br />P.10 <br />t <br />Werk0Mer. 0605149 <br />EPA MoUnd: SWUM <br />raKtractlon: SW3886C <br />Bat M0131030 <br />GOIKIW 80(nWe 10: 0409049.1 03A <br />Maly% <br />(Semple <br />mWXg <br />Spiked <br />mg1Kg <br />M9 <br />% ROc. <br />MSD <br />% Ree. <br />M84AD <br />% RPD <br />LCB <br />% Roo. <br />1030• <br />% Roc <br />LC9•Lt",SO <br />Y. RPb <br />Accaptenoe Crlta is (N,) <br />MS ! MSC LC: 1 xa ci <br />Aeesugrltdrcne <br />TtR <br />2 <br />S51 <br />80,1 <br />I .[ l <br />$6.5 <br />86.6 <br />0.220 <br />30 -130 <br />r <br />31 • 139 <br />4•CatNro•3 bene! <br />ND <br />4 <br />91 <br />81,2 <br />0.216 <br />92.7 <br />96.3 <br />3.19 <br />30 . ISO <br />31 • 134 <br />2.t:7rlsrxlphetiW <br />WD <br />4 <br />$9.6 <br />89 <br />01677 <br />57.9 <br />97.3 <br />0.709 _ <br />10 • 130 <br />31 -134 <br />1.4biohloroptslzetle <br />ND <br />2 <br />58.5 <br />$8.2 <br />0.317 <br />98.6 <br />5^.1 <br />1 A3 <br />"-130 <br />31 . t 84 <br />3t4.ONnitaetaNt fw <br />4a�11ka1fAm01 _ <br />ND <br />IND <br />% <br />d <br />95.6 <br />12.6 <br />91 <br />t2.1 <br />(Al <br />0.593 <br />104 <br />97.8 <br />1.04 <br />94.7 <br />0 <br />3.17 <br />30 - 130 <br />30 • 170 <br />31 -134 <br />31 -184 <br />N T4Ntrecadi.ts.ptnpylarnlne <br />penwhlmphenolry <br />ND <br />N0 <br />2 <br />4 <br />lit <br />19.9 _ <br />1'15 <br />80.9 <br />0 <br />2.40 <br />94.2 <br />$2.4 <br />94.9 <br />53.6 <br />O.S93 <br />139 <br />30-00 <br />30.1:10 <br />31 •130 <br />31 -130 <br />Phenol <br />NA <br />4 <br />81 7 <br />110.4 <br />01966 <br />19.4 <br />511 <br />7.02 <br />30-130 <br />31 • 170 <br />Pyesis <br />~ <br />Nb <br />2 <br />96.2 <br />87.9 <br />2,Oa <br />17.1 <br />96.1 <br />OAP <br />3D - 130 <br />31 -I" <br />- <br />1,1,4-7hichIambd47M4 <br />NO <br />2 <br />98.7 <br />1 $8.4 <br />0.191 <br />9G <br />44.) <br />1,98 <br />M • 130 <br />31 • 110 <br />4541 <br />%SSZ: <br />94 <br />97 <br />200 <br />100 <br />96 <br />99 <br />94 <br />t9 <br />L38 <br />0 <br />96 <br />101 <br />97 <br />101 <br />1.17 <br />0 <br />30 • 130 <br />30-130 <br />3t -130 <br />3( - 130 <br />9bS53: <br />93 <br />200 <br />l 11 <br />111 <br />0 <br />116 <br />114 <br />1.75 <br />30 • 130 <br />3( .130 <br />%S94: <br />80 <br />200 <br />92 <br />1,Ok <br />2,02 <br />96 <br />116 <br />86 <br />(16 <br />0 <br />0 <br />30 •130 <br />30 -110 <br />3(• 130 <br />7( -130 <br />94S45s RO 200 106 <br />%SS6: <br />es <br />200 <br />R4'^- <br />-91 <br />2.60 <br />90 <br />90 <br />0 <br />30.130 <br />�3(-t30 <br />All tarl:tst comyounds to die idood 0lank of this cdruotran butch wCM ND love. then the mc$10d RL with the fatl0w1n$ e:iG4ptions: <br />NONE <br />B61Ct•121530 Su w M= <br />Samoa ID Dole gminpled Date Extracted Dete Analyzed S9mple ID 0ete Sempled oho Lftecfad Date Alt tlywi <br />06415149.001.4 _ 5+D8M64:3QAW" S/0$!00 3109106617nsvt <br />MS ■ Mairlt pike; M ■ morw Spike Duplicate; LCS = Labaretary Control 3"tw L0111,01 a I.s70retDly Gonbol Swiiptn DkV1mt6: APD a %Wve Hifi( 09Aetig ,, <br />Recarety=100' (MS450m0D)1(ARlasnl Sptked); RPD a 106'(W- MM(Mg- ((Mg • MSD)12). <br />VS I MSP spite reeDWn as and ! or W%PD (nay toil etaide Of lnboretary aoasWW n64 0061% due b orae 0r may Of 1110 1090Wleg tel 660PS: e) the WM N rAffmOrK 9a AND <br />conlalnl slflfdficsnl tlerl0entfa9cdlt ®) etlag4a 1WNW9 to til® ■mown Spiked, orb) the vpgwdearrtpiny matrlit I nleftme *IN dw Kpike 0tmw wry, <br />NfA a nstenpuah s9mple b periwm smirk sptka wo Msir(K spike skrplo®te. <br />NR s atttdyte cancarMtstNA 1A na noc, oAovi da spike amount for cell matrk of eKwds br coke ®mer m forwelor malriK or wrnple dUated due to nttn rmtrin or ane" owuem <br />lryaurtapats tlutited eu: of reha0; b ■ lewvr no nwwN e1 suno90 a or tomot nnaMen aro b matrix int■rfgmmem <br />LLtoln sielmoM sgIvm(g sudi lil aMem cHadds end scatarrs = Ocaselmllya rut s+omnn+pd t} nk Ot NW lewis <br />DHS Ccrtificetiun No, 1644 QA/QC C fftcer <br />