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110 2nd Avenue South, #137, Pacheco, CA 94553-5560 <br />124 1 MCCAMPBELL ANALYTICAL INC. Telephone: 925-798-1620 Fax: 925-798-1622 <br />://www.mccau2oell,com E-mail: main@mccampbell.com <br />Cambria Environmental Technology <br />1144 65thStreet, Suite C <br />Oakland, CA 94608 <br />Client Project ID: Chevron- <br />Stockton <br />Date Sampled: 02/09/01 <br />Date Received: 02/09/01 <br />Client Contact: John Riggi <br />Date Extracted: 02/09/01 <br />Client P.O: <br />Date Analyzed: 02/09-02/10/01 <br />7 Oxygenated Volatile Organics By GC/MS <br />EPA method 8260 modified <br />Lab ID <br />59833 <br />59834 59835 <br />Reporting Limit <br />Client ID <br />D-4-3.5 <br />D-5-4 D-6-4 <br />Matrix <br />S <br />S S <br />S <br />W <br />Compound <br />Concentration* <br />ug/kg <br />ug/L <br />Di -isopropyl Ether (DIPS) <br />ND <br />ND <br />ND <br />5.0 <br />1.0 <br />Ethyl tert-Butyl Ether (ETBE) <br />ND <br />ND <br />ND <br />5.0 <br />1.0 <br />Methyl-tert Butyl Ether (MTBE) <br />5.6"' <br />ND <br />ND <br />5.0 <br />1.0 <br />tert-Amyl Methyl Ether (TAME) <br />ND <br />ND <br />ND <br />5.0 <br />1.0 <br />tert-Butanol <br />ND <br />ND <br />ND <br />25 <br />5.0 <br />Methanol <br />ND <br />ND <br />ND <br />1000 <br />200 <br />Ethanol <br />ND <br />ND <br />ND <br />250 <br />50 <br />Surrogate Recoveries (%) <br />Dibromofluoromethane <br />102 <br />102 <br />102 <br />Comments: <br />* water samples are reported in ug/L, soil and sludge samples in ug/kg, wipes in ug/wipe and all TCLP / STLC / SPLP extracts in ug/L <br />ND means not detected above the reporting limit; N/A means surrogate not applicable to this analysis <br />(h) lighter than water immiscible sheen is present; (i) liquid sample that contains greater than —5 vol. % sediment; 0) sample diluted due to <br />high organic content <br />DHS Certification No. 1644 Edward Hamilton, Lab Director <br />