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SAN aOAQLJIN Ar_j HMAXrri-I I:>1S9M1r_"rr <br />TANK CLOSURE PLAN REVIEW CHECKLIST - MINIMUM VERIFICATION LAB ANALYSES <br />TANK <br />ID # <br />TANK CONTENTS TPH-G <br />Waste Product GC -FID <br />(5030) <br />LEADED GASOLINE <br />TPH-D <br />GC -FID <br />(5030) <br />TEPH <br />(3550) <br />(3540) <br />BTX&E <br />(8020) <br />CL HC <br />(8010) <br />(8240) <br />TEL <br />(D <br />EDB <br />0 H S) <br />METALS <br />(ICP- <br />AES) <br />PCB <br />(8270) <br />( 8080 ) <br />TEPH <br />BTX & E (8020) <br />Total Extractable Petroleum Hydrocarbon (8015) <br />UNI, GASOLINE <br />Benzene, Toluene, Xylene & Ethyl Benzene (8020) <br />Chlorinated Hydrocarbon 8010 or 8240 <br />TEL (DOHS-LUFT) <br />Tetraethyl Lead (DOHS-LUFT) <br />EDB (DOHS -AB 1803) <br />GC FID <br />Ethylene dibromide (DOHS -AB 1803) <br />ICP -AES OR AA <br />Gas Chromatography Flame Ionization Detector <br />grouple <br />Inductively ea Plasma Atomic Emission Spectrometry or Atomic <br />Absorption Spectrometry <br />DIESEL <br />Purge and Trap Sample Preparation <br />Sonication Sample Preparation <br />Method 3540 <br />OA/OC <br />Soxhlet Sample Preparation <br />Quality Assurance/Quality Control <br />Notes: To avoid false positive detection of benzene, benzene -free solvents are to be used. <br />Fused capillary columns are preferred to packed columns; a packed column may be used as a <br />"first "dirty" <br />cut" with <br />proper QA/QC is followed. <br />samples or once the hydrocarbons have been characterized and <br />For Drinking Vater Sources EPA recommends that the 500 series for volatile <br />organics be used in preference to the 600 <br />KEROSENE <br />series because the detection limits are lower and <br />UNKNOWN FUEL <br />OIL <br />CHLOR. SOLVENTS <br />NONCHLOR. SOLVTS <br />. . . . . . . . . . . . . . <br />. ......... . <br />WASTE/USED OIL <br />The following listing of <br />terminology used will be <br />laboratory analyses abbreviations is provided as a guide so that <br />more familiar. <br />described in EPA SW 846, <br />All analyses methods are designated EPA methods as <br />Third Edition. Those methods not found in SW 846, are <br />specifically noted. <br />TPH G <br />TPH D <br />Total Petroleum Hydrocarbon, Gasoline <br />Total Petroleum Hydrocarbon, Diesel <br />TEPH <br />BTX & E (8020) <br />Total Extractable Petroleum Hydrocarbon (8015) <br />CL HC 8010 OR 8240 <br />Benzene, Toluene, Xylene & Ethyl Benzene (8020) <br />Chlorinated Hydrocarbon 8010 or 8240 <br />TEL (DOHS-LUFT) <br />Tetraethyl Lead (DOHS-LUFT) <br />EDB (DOHS -AB 1803) <br />GC FID <br />Ethylene dibromide (DOHS -AB 1803) <br />ICP -AES OR AA <br />Gas Chromatography Flame Ionization Detector <br />grouple <br />Inductively ea Plasma Atomic Emission Spectrometry or Atomic <br />Absorption Spectrometry <br />Method 5030 <br />Method 3550 <br />Purge and Trap Sample Preparation <br />Sonication Sample Preparation <br />Method 3540 <br />OA/OC <br />Soxhlet Sample Preparation <br />Quality Assurance/Quality Control <br />Notes: To avoid false positive detection of benzene, benzene -free solvents are to be used. <br />Fused capillary columns are preferred to packed columns; a packed column may be used as a <br />"first "dirty" <br />cut" with <br />proper QA/QC is followed. <br />samples or once the hydrocarbons have been characterized and <br />For Drinking Vater Sources EPA recommends that the 500 series for volatile <br />organics be used in preference to the 600 <br />the QA/QC is better. <br />series because the detection limits are lower and <br />SITE ADDRESS SWEEPS # <br />CONTRACTOR AP ROVAL DATE <br />