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`I INIINIL-M VERIFICATION LABORATORY ANALYSIS <br /> i <br /> nX YC F.*'^TF_S <br /> TANK TANK TPH-G TPH-D BTX & E CL HC TOTAL NtTBE (MTRF. PCB <br /> # CONTENTS 8015 8015 8020 8010 LEAD 801-70 TRA,D(PF, ICAPI <br /> 8260 8260 8260 8240 7420 8260' AF 81-70 <br /> TAME) or 8080 <br /> 8260 7421 8260 AA <br /> I A , <br /> LEADED GAS XX1 7 X <br /> UNL GAS X X X <br /> DIESEL X X X <br /> KEROSENEX X X <br /> UNK FUEL X I X X X �( <br /> PROD. OIL I X X X <br /> I � <br /> CHLOR. <br /> SOLVENTS X X X <br /> NONCHLOR <br /> SOLVENTS X X I X <br /> W AST E% <br /> USED OIL l X X X X X <br /> X X <br /> All analysis methods are the designated EPA methods described in EPA SW 846, Third Edition. Those methods not found in <br /> SW 846 are specifically noted below, Refer to the "SWRCB LUFT Field Manual", Appendix D (B), Tabic 3-5 out page A20 for <br /> minimum detection limits for motor vehicle fuel (gasoline and diesel). Refer to "Tri-Regional Board Staff Recommendations for <br /> Initial Evaluation and Investigation of UST's" for the waste and motor oil minimum detection limits. <br /> Detection Limits that remain below the MCL, STLC or allowable Limit of the contaminant in question will be accepted, <br /> however laboratory shall utilize the most conservative method. <br /> LABORATORY ANALYSES TER�MINOI.OGY: <br /> TPII-G Total Petroleum Hydroc:arboa. Gasoline. GC/FID (5030) 8015 mod or GC/IVIS 8260 <br /> TPH-D Total Petroleum Hydrocarbon. Diesel, GC/FID(3550). 8015 mod or GC/MS 8260 <br /> BTX & E Benzene. Toluene. Xylene&Ethyl Benzene, GCIPID 8020 or GC/MS 8260 <br /> CL HC Chlorinated Hydrocarbon, GC/HSD 8010, GC/MS 8240 or 8260 <br /> TOTAL LEAD Total lead, AA 7420. AA 7421 or ICP-AES 6010 <br /> OXYGENATES MTBE. ETBE.TAME. DIPS, &TBA GC/MS 8260(For MTBE screen only you may use 8020) <br /> META/S ICRP or AA Inductively Coupled Plasma Atomic.Emission Spectrometry 6010 or Atomic Absorption Spectrometry 7000. <br /> Metals: Cadmium. Chromium III and VI, Lead, Zinc and Nickel. <br /> PCB Polychlorinated Biphenyls, GC/MS 8270 or 8080 <br /> GC-FID Gas Chromatography, Flame Ionization Detection <br /> Method 3050 Acid digestion <br /> Method 3540 Soxhlet sample preparation <br /> Method 3550 Sonication sample preparation, extraction method <br /> Method 5030 Pur,c and trap sample preparation <br /> QA/QC Quality Assuranc_/Quality Control <br /> Notes: To avoid false positive detection of benzene, henzene-tree solvents are to be used. Fused capillary columns arc prcicrrt:d to packed <br /> columns: a packed column may be used as a "first cut" with "dirty" samples or once the hydrocarbons have been characterized and proper <br /> QA/QC is followed. <br /> For drinking water sources. EPA recommends that the 500 scrics for volatile organic should be used in preference to the 600 series because the <br /> detection limits are lower and the QA/QC is better. Samples exhibiting any level of heavy metal contamination may require tUrther analysis. <br /> FHS-EHD recommends holding those samples until disposal is indicated. <br /> EH 23 046 (Revised 08/13/99) Page 8 <br />