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1 <br />1 <br />1 <br />1 <br />1 <br />1 <br />1 <br />1 <br />1 <br />1 • • <br />1 10 Second Avenue South, #137, Pacheco, CA 94553 <br />124 MCCAMPBELL ANALYTICAL INC. Telephone : 510-798-1620 Fax : 510-798-1622 <br />http://www.mccanipbell.com E-mail: main@mccampbell.com <br />Advanced GeoEnvironmental <br />Client Project ID: Certified Grocery <br />I <br />Date Sampled: 09/25-09/26/97 <br />Date Received: 09/30/97 <br />1803 West March Lane, Ste A <br />Client Contact: Bill Little Date Extracted: 09/30/97 <br />Stockton, CA 95207 <br />Client P.O: Date Analyzed: 09/30-10/01/97 <br />Diesel Range <br />(C10 -C23) Extractable Hydrocarbons as Diesel * <br />EPA methods modified 8015, and 3550 or <br />3510; California RNA QCB (SF Bay Region) method GCFID(3550) or GCFID(3510) <br />Lab ID Client ID <br />Matrix TPH(d)' % Recovery <br />Surrogate <br />81289 SPI <br />S 1.6,b 106 <br />81290 <br />SP2 <br />S <br />130,c <br />108 <br />81291 <br />SP3 <br />S <br />60,c <br />93 <br />81292 <br />SP4 <br />S <br />79,a <br />93 <br />81293 <br />SP5 <br />S <br />190,a <br />93 <br />81294 <br />SP6 <br />S <br />27,a <br />93 <br />81295 <br />SP7 <br />S <br />760 ,g,b <br />107 <br />81296 <br />SP8 <br />S <br />5200,a <br />96 <br />81297 <br />TS -1 <br />S <br />ND <br />106 <br />81298 <br />TS -2 <br />S <br />N D <br />106 <br />81299 <br />TS -3 <br />S <br />ND <br />106 <br />Reporting Limit unless otherwise W 50 ug/L <br />stated; ND means not detected above <br />the reporting limit S 1.0 mg/kg <br />*water and vapor samples are reported in ug/L, wipe samples in ug/wipe, soil and sludge samples in mg/kg, and all TCLP / STLC / SPLP <br />extracts in ug/L <br /># cluttered chromatogram resulting in coeluted surrogate and sample peaks, or; Surrogate peak is on elevated baseline, or; surrogate has been <br />diminished by dilution of original extract. <br />'The following descriptions of the TPH chromatogram are cursory in nature and McCampbell Analytical is not responsible for their <br />interpretation: a) unmodified or weakly modified diesel is significant; b) diesel range compounds are significant; no recognizable pattern; c) <br />aged diesel? is significant); d) gasoline range compounds are significant, e) medium boiling point pattern that does not match diesel (?); f) <br />one to a few isolated peaks present; g) oil range compounds are significant; h) lighter than water immiscible sheen is present; i) liquid <br />sample that contains greater than —5 vol. % sediment. <br />DHS Certification No. 1644 <br />//�,/ Edward Hamilton, Lab Director <br />