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10/25/2002 10:36 2094683JA3 FIFTH FLOOR PAGE 05
<br />MINIMUM VERIFICATION LABORATORY ANALYSIS
<br />All analyns me&o& are the deli ted EPA nw6ods described m EPA SW $46, Third Editron. l7ho5e rr ttrods not tonna m aw tsvo are
<br />specifically noted below. Refer to the "S CB LUFT Field Manual", Appendix D (B), Table 3-5 on pave A20 for minirnurn detection
<br />limits for motor vehicle fitel (gasoline and diesel). Refer to "Th -Regional Board Staff Recomnmdations for Initial Evaluation and
<br />Investigation of UM' for the waste and motor oil minimum detectionlimits.et "on Limits that remain below the MCL, STLC or
<br />Allowable Limit of the conte ant in question will be accepted, however laboratory shall utilize the most conservative method.
<br />TPH-G Total Petroleum Hydrocarbon, Gasoline, GCIRD (5030) 8015 mod or GC/MS 8260
<br />TPH-D Total Petroleum Hydrocarbon, Diesel, GC/71D (3550), 8015 mod or OCIMS 8260
<br />BTX & Ebenzene, Toluene, Xytene & Ethyl Benzene, GC/PID 8020 or CC MS 8260
<br />CL HC Chlorinated Hydrocarbon, GC/HSD 8010, GC1MS 8240 or 8260
<br />TOTAL LEAD Total lead, AA 7420, AA 7421 or ICNAES 6010
<br />OXYGENATES MTBE, ETBE, TAME, DIPE, & TBA G0MS 8260 (For MTBE soreeo only you may use 8020)
<br />METALS ICAP or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption Spectrometry 7000. Metals:
<br />Cadwiutts, Cdrot»tum III mad WI, Lead, Zinc and Nickel.
<br />PCB Polychlorinated Biphenyls, GCIMS 8270 or 8080
<br />GC -FID Gas Chromatography, Flame Ionization Detection
<br />Method 3050 Acid digestion
<br />Method 3540 SoxhIct sample preparation
<br />Method 3550 Sonication sample preparation, extraction method
<br />Method 5030 Purge and trap sample preparation
<br />QA/QC Quality AssutancelQu.ality Control
<br />Notes: To avoid false positive detection of benzene, benzene-froe solvents are to be used. Fused capillary column are preferred to packed columna; a
<br />packed column may be used as a "first cut" with "dirty" samples or once the hydrocarbons have been, characterized and proper.QA/QC is followed. For
<br />drinking water sources, EPA recommends that the 500 series for volatile organic should be used in preference to the 600 series because the detection
<br />limits are lower and the QA/QC is better. Samples exhibiting any level of heavy metal contamination may require further analysis. PHS-EHD
<br />recommends holding those samples until disposal is indicated.
<br />EH 23 046 (Revised 05/09/00)
<br />OXYGEN
<br />TANK TANK TPH-G
<br />TPH-D
<br />BTX & E
<br />CL HC TOTAL
<br />MTBE
<br />ATES
<br />METAL
<br />PCB
<br /># CONTI;NI°S 8015
<br />8015
<br />8020
<br />8010 LEAD
<br />9020
<br />(MTBE.
<br />ICAPI
<br />8270
<br />8260
<br />8260
<br />8260
<br />8240 7420
<br />8260
<br />'IBA,DIPE,
<br />AES or
<br />808021 '
<br />8260 7421
<br />TA
<br />AA
<br />8260
<br />LEADED GAS X
<br />X
<br />X
<br />X
<br />UNL GAS X
<br />X
<br />X
<br />DIESEL
<br />X I
<br />X
<br />KEROSENE
<br />x
<br />X
<br />X
<br />UNK FUEL X
<br />X
<br />X
<br />X
<br />X
<br />PROD. ODL
<br />X
<br />X
<br />X
<br />CHLOR,
<br />X
<br />SOLVENTS
<br />X
<br />X
<br />NONCHLOR
<br />X
<br />SOLVENTS
<br />X
<br />X
<br />WASTE\
<br />USED OIL X
<br />X
<br />X
<br />X
<br />X
<br />X
<br />X
<br />All analyns me&o& are the deli ted EPA nw6ods described m EPA SW $46, Third Editron. l7ho5e rr ttrods not tonna m aw tsvo are
<br />specifically noted below. Refer to the "S CB LUFT Field Manual", Appendix D (B), Table 3-5 on pave A20 for minirnurn detection
<br />limits for motor vehicle fitel (gasoline and diesel). Refer to "Th -Regional Board Staff Recomnmdations for Initial Evaluation and
<br />Investigation of UM' for the waste and motor oil minimum detectionlimits.et "on Limits that remain below the MCL, STLC or
<br />Allowable Limit of the conte ant in question will be accepted, however laboratory shall utilize the most conservative method.
<br />TPH-G Total Petroleum Hydrocarbon, Gasoline, GCIRD (5030) 8015 mod or GC/MS 8260
<br />TPH-D Total Petroleum Hydrocarbon, Diesel, GC/71D (3550), 8015 mod or OCIMS 8260
<br />BTX & Ebenzene, Toluene, Xytene & Ethyl Benzene, GC/PID 8020 or CC MS 8260
<br />CL HC Chlorinated Hydrocarbon, GC/HSD 8010, GC1MS 8240 or 8260
<br />TOTAL LEAD Total lead, AA 7420, AA 7421 or ICNAES 6010
<br />OXYGENATES MTBE, ETBE, TAME, DIPE, & TBA G0MS 8260 (For MTBE soreeo only you may use 8020)
<br />METALS ICAP or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption Spectrometry 7000. Metals:
<br />Cadwiutts, Cdrot»tum III mad WI, Lead, Zinc and Nickel.
<br />PCB Polychlorinated Biphenyls, GCIMS 8270 or 8080
<br />GC -FID Gas Chromatography, Flame Ionization Detection
<br />Method 3050 Acid digestion
<br />Method 3540 SoxhIct sample preparation
<br />Method 3550 Sonication sample preparation, extraction method
<br />Method 5030 Purge and trap sample preparation
<br />QA/QC Quality AssutancelQu.ality Control
<br />Notes: To avoid false positive detection of benzene, benzene-froe solvents are to be used. Fused capillary column are preferred to packed columna; a
<br />packed column may be used as a "first cut" with "dirty" samples or once the hydrocarbons have been, characterized and proper.QA/QC is followed. For
<br />drinking water sources, EPA recommends that the 500 series for volatile organic should be used in preference to the 600 series because the detection
<br />limits are lower and the QA/QC is better. Samples exhibiting any level of heavy metal contamination may require further analysis. PHS-EHD
<br />recommends holding those samples until disposal is indicated.
<br />EH 23 046 (Revised 05/09/00)
<br />
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