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Y <br />X <br />SAMPLING PROTOCOL FOR ROUTINE PIPING/DISPENSER REMOVAL/REPLACEMENT <br />The following represents minimum sampling criterion required for closure compliance. Soil samples collected shall be <br />representative of native soils beneath the tank's invert (tank's bottom) at a collection depth not to exceed 2 - 4 feet. If <br />contamination is documented during closure, an Unauthorized Release Notification must be completed and submitted within five (5) <br />working days pursuant to California Health & Safety Code, Section 25295. <br />DISPENSER PIPING AND STOCKPILE SAMPLES <br />DISPENSER SAMPLES 1 Sample beneath each dispenser <br />PIPING SOIL SAMPLES 1 Sample every 20 lineal feet <br />DISPENSER & PIPING STOCKPILE SAMPLES 2 Samples every 50 cubic yards <br />TABLE #2 RECOMMENDED M <br />STC <br />FOR <br />UNDERGROUND <br />TANK TANK <br />TPH-G <br />TPH-D <br />BTX & E <br /># CONTENTS <br />8015 <br />8015 <br />8020 <br />8260 <br />8260 <br />8260 <br />LEADED GAS <br />X <br />X <br />UNL GAS <br />X <br />X <br />DIESEL <br />KEROSENE <br />X <br />X <br />UNK FUEL <br />X <br />X <br />X <br />PROD. OIL <br />X <br />CHLOR. <br />SOLVENTS <br />NONCHLOR <br />SOLVENTS <br />X <br />X <br />WASTE\USED OIL <br />OR <br />X <br />X <br />X <br />UNKNOWN <br />CONTENTS <br />Notes: <br />1. EPA Method 82606 nalyses must include all analytes listed in the method plus fuel oxygenates methy - <br />tertiary -butyl ether TBE), diisopropyl ether (DIPE), ethyl -tertiary -butyl ether (EtBE), tertiary -amyl -methyl <br />ether (TAME), to iary-butanol (TBA), methanol and ethanol and fuel additives 1,2-dichloroethane (1,2 -DCA) <br />and ethylene romide (EDB or 1,2-dibromoethane). <br />If pentachl op <br />(PCP) is identified, analyze the soil and/or water sample for dioxins and furans by EPA <br />Method 8 90 and pesticides by EPA Method 8081 A. <br />METALS ICAP or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption <br />Spectrometry 7000. Metals: Cadmium, Chromium III and VI, Lead, Zinc and Nickel. <br />Non-proprietary, performance based analytical methods may be used with approval of Regional Board staff. <br />Revised 02/20/09 <br />4 <br />