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W110 <br />cCampbell Analytical, Inc. <br />2nd Avenue D7, Pacheco, CA 94553-5560 <br />Telephone: 925-798-1620 Fax:925-798-1622 <br />Website: www.nrxampbell.com Email: main@n=arnpbell.com <br />Shaw Environmental <br />4005 Port Chicago Hwy <br />Concord, CA 94520 <br />Client Project ID: San Joaquin Garage <br />Date Sampled: <br />05/18/04 <br />Date Received: 05/18/04 <br />Client Contact: Rob Delnagro <br />Date Extracted: 05/18/04 <br />Client P.O.: <br />I Date Analyzed: 05/18/04 <br />Oxygenated Volatile Organics by P&T and GC/MS* <br />Extraction Method: SW5030B Analytical Method: SW8260B <br />Work Order. 0405272 <br />Lab ID <br />0405272-OOIA <br />Client ID <br />UP -1 <br />Reporting Limit <br />DF =1 <br />for <br />Matrix <br />S <br />DF <br />-- ..._...---- — ...— <br />1 <br />- - ----- .---- --- ..--------------..... <br />S <br />W <br />Compound <br />Concentration <br />µ8/Kg <br />ug/L <br />tert-Amyl methyl ether (TAME) <br />ND <br />5.0 <br />NA <br />t -Butyl alcohol (TBA) <br />ND <br />25 <br />NA <br />Diisopropyl ether (DIPE) <br />ND <br />5.0 <br />NA <br />Ethyl tert-butyl ether (ETBE) <br />ND <br />5.0 <br />NA <br />Methyl -t -butyl ether (MTBE) <br />ND <br />5.0 <br />NA <br />Surrogate Recoveries (%) <br />—F— <br />%SS: 105 <br />Comments <br />* water and vapor samples and all TCLP & SPLP extracts are reported in gg/L, soil/sludge/solid samples in gg/kg, wipe samples in ltg/wipe, <br />product/oil/non-aqueous liquid samples in mg/L. <br />ND means not detected above the reporting limit; N/A means analyte not applicable to this analysis. <br /># surrogate diluted out of range or surrogate coelutes with another peak- <br />eakh) lighter than water immiscible sheen/product is present; i) liquid sample that contains greater than —1 vol. % sediment; j) sample diluted due to high <br />h) <br />organic content. <br />DHS Certification No. 1644 <br />Angela Rydelius, Lab Manager <br />