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May 19 2004 3:47PM 11,igiAMPBELL ANALYTICAL INC 92' 84612 P.5 <br />W Ir <br />McCampbell AnalyticaL Inc. <br />110 2nd Avenor South, #D7, Pacheco, CA 94553-5560 <br />Telephone; 925-799-1620 Fax : 925-7984622 <br />I <br />A# <br />Website: www,n=aimpbeg.com E-rodl; nain@m=anpbcl.com <br />Shaw Environmental <br />Client Project ID: San Joaquin Garage <br />Date Sampled: 05/18104 <br />4005 Port Chicago Hwy <br />Date Received: 05/18/04 <br />Client Contact: Rob Dclnagro <br />Date Extracted: 05/18/04 <br />Concord, CA 94520 <br />Client P.O.: :Date <br />Analyzed: 05/18/04 <br />Oxygenated Volatile Organics by P&T and GC/MS* <br />Extraction Method SW5030B Analytical Method: SW826011 Work Order: 04405272 <br />Lab ID <br />0405272-001A <br />Client ID <br />UP-] <br />Reporting Limit for <br />DF —1 <br />Matrix <br />S <br />DF <br />I <br />S W <br />Compound <br />Concentration <br />pg/Kg ug/L <br />tert-Amyl methyl ether (TAME) <br />ND <br />5.0 NA <br />t -Butyl alcohol (TBA) <br />ND <br />25 NA <br />Diisopropyl other (RIPE) <br />ND <br />5.0 NA <br />Ethyl tert-butyl ether (EYBE) <br />ND <br />5.0 NA <br />Medivi-t.butyl ether (MTBE) <br />ND <br />5.0 NA <br />Surrogate Recoveries <br />%SS: <br />105 <br />Comments <br />J* water and vapor samples and all TCLP & SPLP extracts are reported in Agg, soil/sludge/solid samples in jig/kg, wipe samples in pg/wipe, <br />product/oil/non-aqueous liquid samples in mg/L- <br />ND means not detected above the reporting limit, N/A means analyte not applicable to this analysis. <br /># surrogate diluted out of range or surrogate coclutes with another peak <br />h) lighter than water immiscible sheen/product is present; i) liquid sample that contains greater than —1 vol. % sediment; j) sample diluted due to high <br />12mic content. <br />DHS Certification No. 1644 <br />A- Angela Rydelius, Lab Manager <br />