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Jul 01 03.11:32a TAIT Environmental System () 858-1011 p.6
<br />06/39/2003 12:06 2H 83433 FIFTH FLOOR PAGE 06
<br />MINIMUM VERIFICATION LABORATORY ANALYSIS
<br />specifically noted below. Refer to the "SWRCB LUFT Field Manual", Appendix D (B), Table 3-5 on page A20 for minimum detection
<br />limits for motor vehicle fuel (gasoline and diesel). Refer to '"Tri -Regional Board Staff Recommendations for initial Evaluation and
<br />Investigation of UST's" for the waste and motor oil tninimuun detection limits. Detection Limits that remain below the MCL, STLC or
<br />Allowable Limit of the contaminant in question will be aecepted, however laboratory shall utilize the most eouservadve metbod.
<br />LABORATORY ANALYSLS TERMINOLOGY:
<br />TPH-G Total Petroleum Hydrocarbon, Gasoline, QC/FID(5030) 8015 mod or GCIMS 8260
<br />17H -D Total Petroleum Hydrocarbon, Diesel, GC/T'10 (3550), 8015 mod or GUMS 8260
<br />BTX & EBenzenc, Toluene, Xylenc & Ethyl Benzcne, GC/PID 8020 or GUMS 8260
<br />CL HC Chlorinated Hydrocarbon, GOHSD 8010, OCIMS 8240 or 8260
<br />TOTAL LEAD Total lead, AA 7420, AA 7421 or ICP -AES 6010
<br />OXYGENATES MTBE, UK, 'I AML, D1PE, & 'FBA GUMS 8260 (For MTBE ecrc� you may use 8020)
<br />METALS ICRP or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption Spectiomerry7000. Metals'
<br />Cadmium, Chromium III and VI, Lead, Zinc. and Nickel.
<br />PC8 Polychlorinated Biphenyls, GC1MS 8270 or 8080
<br />GC-F]D Gas Chromatography, Flame Ionization Detection
<br />Method 3050 Acid digestion
<br />Method 3540 Soxhlet sample preparation
<br />Mcthod 3550 Sonication sample preparation, extraction method
<br />Method 5030 Purge and trap sample preparation
<br />QA/QC Quality Assurance/Quality Control
<br />Notes; To avoid false positive detcetion of benzene, benzene -free solvents arc to be used. Fused capillary columns are preferred to packed columns; a
<br />packed column may be used as a "first cot" with "dirty" samples or once the hydrocarbons have been characterized acrd proper QA/QC is followed. For
<br />drinking water sources, EPA recommends that the 500 series for volatile organic should be used in preference to the 600 series because the detection
<br />limits are tower and the QA/QC is better. Samples exhibiting any level of heavy metal contamination may require further analysis. PNS.FHD
<br />recommends holding those samples unfit disposal is indicated.
<br />EH 23 046 (Revised 05/04/00)
<br />OXYGEN'
<br />TANK.
<br />TANK
<br />TPH-G
<br />TPH-i')
<br />BTX & E
<br />CL HC
<br />TOTAL
<br />MTBE
<br />ATES
<br />ME''"c
<br />PCB
<br />#
<br />CONTENTS
<br />8015
<br />801.5
<br />8020
<br />8010
<br />LEAD
<br />8020
<br />(MTBE.
<br />ICAp/
<br />8270
<br />8260
<br />8260
<br />8260
<br />8240
<br />7420
<br />8260
<br />TBA.D(PE.
<br />ETRE,
<br />AES or
<br />8080
<br />8260
<br />7421
<br />TAME)
<br />AA
<br />8260
<br />LEADED GAS
<br />X
<br />X
<br />X
<br />X
<br />UNL GAS
<br />X
<br />%C
<br />X
<br />DIESEL
<br />X
<br />?C
<br />KEROSENE
<br />X
<br />X
<br />X
<br />UNK FUEL
<br />X
<br />X
<br />X
<br />X
<br />X
<br />PROD. OIL
<br />X
<br />X
<br />X
<br />CHLOR.
<br />X
<br />SOLVENTS
<br />X
<br />NONCHLOR
<br />�X
<br />X
<br />SOLVENTS
<br />X X
<br />WASTE\
<br />USED OIL
<br />X
<br />X X
<br />X
<br />X
<br />X X
<br />All analvsis
<br />methods are the
<br />designated FPA
<br />methods described in EPA
<br />SW 846. Third Edition.
<br />Those methods not
<br />found in SW 846 are
<br />specifically noted below. Refer to the "SWRCB LUFT Field Manual", Appendix D (B), Table 3-5 on page A20 for minimum detection
<br />limits for motor vehicle fuel (gasoline and diesel). Refer to '"Tri -Regional Board Staff Recommendations for initial Evaluation and
<br />Investigation of UST's" for the waste and motor oil tninimuun detection limits. Detection Limits that remain below the MCL, STLC or
<br />Allowable Limit of the contaminant in question will be aecepted, however laboratory shall utilize the most eouservadve metbod.
<br />LABORATORY ANALYSLS TERMINOLOGY:
<br />TPH-G Total Petroleum Hydrocarbon, Gasoline, QC/FID(5030) 8015 mod or GCIMS 8260
<br />17H -D Total Petroleum Hydrocarbon, Diesel, GC/T'10 (3550), 8015 mod or GUMS 8260
<br />BTX & EBenzenc, Toluene, Xylenc & Ethyl Benzcne, GC/PID 8020 or GUMS 8260
<br />CL HC Chlorinated Hydrocarbon, GOHSD 8010, OCIMS 8240 or 8260
<br />TOTAL LEAD Total lead, AA 7420, AA 7421 or ICP -AES 6010
<br />OXYGENATES MTBE, UK, 'I AML, D1PE, & 'FBA GUMS 8260 (For MTBE ecrc� you may use 8020)
<br />METALS ICRP or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption Spectiomerry7000. Metals'
<br />Cadmium, Chromium III and VI, Lead, Zinc. and Nickel.
<br />PC8 Polychlorinated Biphenyls, GC1MS 8270 or 8080
<br />GC-F]D Gas Chromatography, Flame Ionization Detection
<br />Method 3050 Acid digestion
<br />Method 3540 Soxhlet sample preparation
<br />Mcthod 3550 Sonication sample preparation, extraction method
<br />Method 5030 Purge and trap sample preparation
<br />QA/QC Quality Assurance/Quality Control
<br />Notes; To avoid false positive detcetion of benzene, benzene -free solvents arc to be used. Fused capillary columns are preferred to packed columns; a
<br />packed column may be used as a "first cot" with "dirty" samples or once the hydrocarbons have been characterized acrd proper QA/QC is followed. For
<br />drinking water sources, EPA recommends that the 500 series for volatile organic should be used in preference to the 600 series because the detection
<br />limits are tower and the QA/QC is better. Samples exhibiting any level of heavy metal contamination may require further analysis. PNS.FHD
<br />recommends holding those samples unfit disposal is indicated.
<br />EH 23 046 (Revised 05/04/00)
<br />
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