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1 <br />W.O. Sample Matrix: Soil <br />i <br />i <br />QC SUMMARY REPORT FOR SW8015B <br />QC Matrix: Soil BatchlD: 63491 WnrknrdPr 1119559 <br />EPA Method: SW8015B <br />Extraction: SW3550B <br />BATCH 63491 SUMMARY <br />M C <br />p <br />a Pl 1 b 11 Anal <br />a I <br />Inc. <br />Analyte <br />1534 Willow Pass Road CA 94565-1701 <br />Toll Free Telephm: (877) 252-9262 / Fax: (925) 252-9269 <br />Sample <br />"When nity Counts <br />MS <br />MSD <br />MS -MSD <br />http://www.nmeampbeH.com / E-mail: p bell.com <br />1 <br />W.O. Sample Matrix: Soil <br />i <br />i <br />QC SUMMARY REPORT FOR SW8015B <br />QC Matrix: Soil BatchlD: 63491 WnrknrdPr 1119559 <br />EPA Method: SW8015B <br />Extraction: SW3550B <br />BATCH 63491 SUMMARY <br />Spiked Sample ID: <br />1112484-005A <br />Analyte <br />Date Analyzed Lab ID <br />Sample <br />ISpiked <br />MS <br />MSD <br />MS -MSD <br />LCS <br />Acceptance Criteria (%) <br />mg/Kg % Rec.% Rec. % RPD % Rec. MS / MSD RPD <br />LCS <br />TPH-Diesel (CIO -C23) <br />12/20/11 2:00 AIS <br />ND <br />40 <br />122 <br />122 <br />0 <br />107 <br />70-130 30 <br />70-130 <br />%SS: <br />94 <br />25 <br />108 <br />108 <br />0 <br />97 <br />70-130 30 <br />70- <br />0-All <br />AHtarget compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: <br />NONE <br />MS = Matrix Spike; MSD = Matrix Spike Duplicate; LCS = Laboratory Control Sample; LCSD = Laboratory Control Sample Duplicate; RPD = Relative Percent Deviation. <br />% Recovery = 100' (MS -Sample) / (Amount Spiked); RPD = 100' (MS - MSD) / ((MS + MSD) / 2). <br />MS / MSD spike recoveries and / or %RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons: a) the sample is inhomogenous AND contains <br />significant cencenhations of analyte relative to the amount spiked, or b) the spiked sample's matrix interferes with the spike recovery. <br />PYA not enough sample to perform matrix spike and matrix spike duplicate. <br />NR = analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. <br />DHS FLAP Certification 1644 <br />QA/QC Officer <br />Page 23 of 23 <br />BATCH 63491 SUMMARY <br />Lab ID <br />Date Sampled <br />Date Extracted <br />Date Analyzed Lab ID <br />Date Sampled Date Extracted <br />Date Analyzed <br />1112555-OOIA <br />12/19/11 <br />12/19/11 <br />12/19/11 10:38 PM <br />1112555-002A <br />12/19/11 12/19/11 <br />12/20/11 2:00 AIS <br />1112555-003A <br />12/19/11 <br />12/19/11 <br />12/20/11 12:53 AM <br />1112555-004A <br />12/19/11 12/19/11 <br />12/20/11 5:21 AN <br />1112555-005A <br />12/19/11 <br />12/19/11 <br />12/20/117:35 AM <br />MS = Matrix Spike; MSD = Matrix Spike Duplicate; LCS = Laboratory Control Sample; LCSD = Laboratory Control Sample Duplicate; RPD = Relative Percent Deviation. <br />% Recovery = 100' (MS -Sample) / (Amount Spiked); RPD = 100' (MS - MSD) / ((MS + MSD) / 2). <br />MS / MSD spike recoveries and / or %RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons: a) the sample is inhomogenous AND contains <br />significant cencenhations of analyte relative to the amount spiked, or b) the spiked sample's matrix interferes with the spike recovery. <br />PYA not enough sample to perform matrix spike and matrix spike duplicate. <br />NR = analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. <br />DHS FLAP Certification 1644 <br />QA/QC Officer <br />Page 23 of 23 <br />