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RI <br /> 1534Willow Pass Road,Pi CA 94565-1701 <br /> M c CamobeII Ar'a 1C a I• n C Toll Free Telephone:(877)252-9262/Fax:(925)252-9269 <br /> Ff"en Q=14 COuiW�r http://www.mccaropbell.com/E-mail:viain@mccampbell.com <br /> QC SUMMARY REPORT FOR SW8082 <br /> W.O.Sample Matrix: Soil QC Matrix: Soil BatchlD:63416 WorkOrder. 1112398 <br /> EPA Method: SW8082 Extraction: SW3550B Spiked Sample ID: 1112398-007A <br /> Analyte Sample Spiked MS MSD MS-MSD LCS Acceptance Criteria(%) <br /> mg/kg mg/kg %Rec. %Rec. %RPD %Rec. MS/MSD RPD LCS <br /> Aroclor1260 ND 0.15 91.9 89.7 2.33 96.8 70-130 20 70-130 <br /> %SS.' 1 100 0.050 125 116 1 7.64 77 1 70-130 20 70-130 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: <br /> NONE <br /> BATCH 63416 SUMMARY <br /> Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date Extracted Date Analyzed <br /> 1112398-001A 12/13/11 1:45 PM 12/13/11 12/14/115:06 PM 1112398-OOIA 12/1.3/11 1:45 PM 12/13/11 12/14/115:06 PM <br /> 1112398-002A 12/13/112:24 PM 12/13/11 12/14/114:58 PM 1112398-003A 12/13/112:05 PM 12/13/11 12/'14/114:10 PM <br /> 1112398-003A 12/13/112:05 PM 12/13/11 12/14/114:10 PM 1112398-004A 12/13/112:40 PM 12/13/11 12/14/112:20 PM <br /> 11 12398-004A 12/13/112:40 PM 12/13/11 12/14/112:20 PM 11 12398-005A 12/13/11 2:45 PM 12/13/11 12/14/113:15 PM <br /> 1112398-005A 12/13/11 2:45 PM 12/13/11 12/14/113:15 PM 1112398-006A 12/13/112:50 PM 12/13/11 12/14/114:58 PM <br /> 1112398-007A 12/13/11 3:08 PM 12/13/11 12/14/112:12 PM <br /> i <br /> MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative Percent Deviation. <br /> %Recovery=100'(MS-Sample)/(Amount Spiked);RPD=100"(MS- MSD)/((MS+MSD)/2). <br /> MS/MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons:a)the sample is inhomogenous AND contains <br /> significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> N/A=not enough sample to perform matrix spike and matrix spike duplicate. <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. ' <br /> #su ate diluted out of range or sungate ooelutes with another nk. <br /> DHS ELAP Certification 1644 QA/QC Officer <br /> r <br /> Page 18 of 22 <br />