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IQC SUMMARY REPORT FOR SW8260B <br />M <br />W.O. Sample Matrix: Soil QC Matrix: Soil BatchlD: 63413 <br />WorkOrdec 1119399 <br />EPA M : SW8260B <br />Extraction: SW5030B <br />12/111111:01 PM <br />12/13/11 <br />12/14/11 1:51 AM <br />MA <br />Yt C <br />q <br />m e� I AnQ' <br />ei I <br />n C • <br />Analyte <br />1534 Willow Pass Road, " CA 94565-1701 <br />Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 <br />qSpiked <br />119%eft Counft t' <br />MSD <br />% Rec. <br />MS -MSD <br />% RPD <br />LCS <br />% Rec. <br />bup://www.mccampbeH.com / E-mail: main@mccampbellcorn <br />IQC SUMMARY REPORT FOR SW8260B <br />M <br />W.O. Sample Matrix: Soil QC Matrix: Soil BatchlD: 63413 <br />WorkOrdec 1119399 <br />EPA M : SW8260B <br />Extraction: SW5030B <br />12/111111:01 PM <br />12/13/11 <br />12/14/11 1:51 AM <br />11 12199-002A 12/13/11 3:20 PM 12/13/11 12/14/112:29 A1% <br />spiked sample ID: <br />1112388-019A <br />Analyte <br />Sample <br />mg/Kg <br />qSpiked <br />MS <br />% Rec. <br />MSD <br />% Rec. <br />MS -MSD <br />% RPD <br />LCS <br />% Rec. <br />Acceptance Criteria (%) <br />MS / MSD RPD LCS <br />tern -Amyl methyl ether (TAME) <br />ND <br />102 <br />91.7 <br />11.0 <br />103 <br />70-130 <br />30 <br />70-130 <br />Benzene <br />ND <br />0.050 <br />111 <br />97.5 <br />13.1 <br />114 <br />70-130 <br />30 <br />70-130 <br />t -Butyl alcohol (TBA) <br />ND <br />0.25 <br />74 <br />77.1 <br />4.05 <br />74.6 <br />70-130 <br />30 <br />70-130 <br />Chlorobenzene <br />ND <br />0.050 <br />105 <br />91.5 <br />13.3 <br />107 <br />70-130 <br />30 <br />70-130 <br />1,2-Dibromoethane (EDB) <br />ND <br />0.050 <br />95.9 <br />84.2 <br />13.0 <br />96.3 <br />70-130 <br />30 <br />70-130 <br />1,2-Dichloroethane (1,2 -DCA) <br />ND <br />0.050 <br />104 <br />90.1 <br />14.0 <br />105 <br />70-130 <br />30 <br />70-130 <br />IJ-Dichloroethene <br />ND <br />0.050 <br />112 <br />97.5 <br />13.7 <br />113 <br />70-130 <br />30 <br />70-130 <br />Diisopropyl ether (DIPS) <br />ND <br />0.050 <br />109 <br />95.9 <br />12.9 <br />112 <br />70-130 <br />30 <br />70-130 <br />Ethyl tert-butyl ether (ETBE) <br />ND <br />0.050 <br />94.3 <br />83.8 <br />11.8 <br />94.5 <br />70- 130 <br />30 <br />70-130 <br />Methyl -t -butyl ether (MTBE) <br />ND <br />0.050 <br />99.7 <br />88 <br />12.5 <br />99.2 <br />70-1130 <br />30 <br />70-130 <br />Toluene <br />ND <br />0.050 <br />109 <br />96.1 <br />12.2 <br />112 <br />70-130 <br />30 <br />70-130 <br />Trichloroethene <br />ND <br />0.050 <br />107 <br />93.1 <br />13.5 <br />110 <br />70-130 <br />30 <br />70-130 <br />%SSl: <br />111 <br />0.12 <br />118 <br />118 <br />0 <br />117 <br />70-130 <br />30 <br />70-130 <br />%SS2: <br />119 <br />0.12 <br />118 <br />117 <br />0.762 <br />118 <br />70 -130 <br />30 <br />70-130 <br />%SS3: <br />100 <br />0.012 <br />103 <br />102 <br />1.47 <br />98 <br />1 70-130 <br />3070 <br />-130 <br />All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: <br />NONE <br />BATCH 63413 SUMMARY <br />Lab ID Date Sampled Date Extracted Date Analyzed Lab ID <br />Date Sampled Date Extracted Date Analyzed <br />® MS = Matrix Spike MSD = Matrix Spike Duplicate; LCS = Laboratory Control Sample; LCSD = Laboratory Control Sample Duplicate; RPD = Relative Percent Deviation. <br />% Recovery =100 " (MS -Sample) / (Amount Spiked); RPD =100 ' (MS - MSD) / ((MS + MSD) / 2). <br />'MS / MSD spike recoveries and / or %RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons: a) the sample is inhomogenous AND contains <br />significant concentrations of analyte relative to the amount spiked, or b) the spiked sample's matrix interferes with the spike recovery. <br />N/A = not enough sample to perform matrix spike and matrix spike duplicate. <br />NR = analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content <br />La solvents such as meth ene chloride and acetone may occasionally appear in the method blank at low levels. <br />DHS FLAP Certification 1644 <br />11 1 QA/QC Officer <br />Page 17 of 20 <br />1112399-OOIA <br />12/111111:01 PM <br />12/13/11 <br />12/14/11 1:51 AM <br />11 12199-002A 12/13/11 3:20 PM 12/13/11 12/14/112:29 A1% <br />1112399-003A <br />12/13/11 3:30 PM <br />12/13/11 <br />12/14/113:07 AM <br />1112399-004A 12/13/113:40 PM 12/13/11 12/14/113:47 AI` <br />1112399-OOSA <br />12/13/113:55 PM <br />12/13/11 <br />12/14/114:26 AM <br />® MS = Matrix Spike MSD = Matrix Spike Duplicate; LCS = Laboratory Control Sample; LCSD = Laboratory Control Sample Duplicate; RPD = Relative Percent Deviation. <br />% Recovery =100 " (MS -Sample) / (Amount Spiked); RPD =100 ' (MS - MSD) / ((MS + MSD) / 2). <br />'MS / MSD spike recoveries and / or %RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons: a) the sample is inhomogenous AND contains <br />significant concentrations of analyte relative to the amount spiked, or b) the spiked sample's matrix interferes with the spike recovery. <br />N/A = not enough sample to perform matrix spike and matrix spike duplicate. <br />NR = analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content <br />La solvents such as meth ene chloride and acetone may occasionally appear in the method blank at low levels. <br />DHS FLAP Certification 1644 <br />11 1 QA/QC Officer <br />Page 17 of 20 <br />