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QC SUNBIARY REPORT FOR E218.6m 0 <br />W.O. Sample Matrix: Soil QC Matrix: Soil BatchlD: 63486 WorkOrder: 1112484 <br />EPA Method: E218.6 on: SW3060A Spiked Sample ID: 1112398-001A <br />Analyte Sample Spiked MS <br />mg/Kg mg/Kg % Rec. <br />MSD <br />MS -MSD LCS Acceptance Criteria ("�) <br />MCCamgbell <br />--- <br />, AnQI r�iCal <br />inc.oll <br />I <br />1534 Willow Pass Road, Pitts CA 94565-1701 <br />Free Telephone: (877) 252-9262 / Fax. (925) 252-9269 <br />rrlfken <br />Counft" <br />12/15/11 11:45 AM <br />12/19/11 <br />httpJ/www.mccampbeR.com/Email:mainQmccampbelLcom <br />QC SUNBIARY REPORT FOR E218.6m 0 <br />W.O. Sample Matrix: Soil QC Matrix: Soil BatchlD: 63486 WorkOrder: 1112484 <br />EPA Method: E218.6 on: SW3060A Spiked Sample ID: 1112398-001A <br />Analyte Sample Spiked MS <br />mg/Kg mg/Kg % Rec. <br />MSD <br />MS -MSD LCS Acceptance Criteria ("�) <br />% Rec. <br />% RPD % Rec. MS / MSD RPD LCS <br />Hexachrome ND 400 113 <br />114 <br />0.792 104 1 70-130 20 80-120 <br />All target compounds in the Method Blank of this extraction batch were ND less than the method RL With the following exceptions: <br />NONE <br />BATCH 63486 SUMMARY <br />Lab ID Date Sampled Date Extracted Date Analyzed Lab ID <br />Date Sampled Date Extracted Date Analyzed <br />1112484-001A <br />12/15/11 10:45 AM <br />12/19/11 <br />12/19/117:57 PM <br />11 12484-002A 12/15/11 11:00 AM 12/19/11 12/19/118:16 PM <br />1112484-003A <br />12/15/11 11:25 AM <br />12/19/11 <br />12/19/118:34 PM <br />1112484-004A 12/15/11 11:35 AM 12/19/11 12/19/118:52 PM <br />1112494-005A <br />12/15/11 11:45 AM <br />12/19/11 <br />12/19/119:11 PM <br />MS = Matrix Spike; MSD = Matrix Spike Duplicate; LCS = Laboratory Control Sample; LCSD = Laboratory Control Sample Duplicate; RPD = Relative Percent Deviation. <br />% Recovery = 100' (MS -Sample) / (Amount Spiked); RPD = 100 ^ (MS - MSD) / ((MS + MSD) / 2). <br />MS / MSD spike recoveries and / or %RPD may fall outside of laboratory acceptance criteia due to one or more of the following reasons: a) the sample is inhomogenous AND contains <br />significant concentrations of analyte relative to the amount spiked, or b) the spiked sample's matrix interferes with the spike recovery. <br />N/A = not applicable to this method. <br />NR = analyte concentration in sama exceeds sDike amount for soil matrix or exceeds 2x spike amount for water matt or sample diluted due to high matrix or analvte content. ' <br />DHS ELAP Certification 1644 <br />QA/QC Officer <br />r <br />Pae 16 of 21 <br />