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QCBatchlD: QC1200185 Analyst: Jarriaga Method: EPA 8270C Matrix: Solid Analyzed: 03/25/2019 Instrument: SVOA-MS(group) Blank Analyte Result Units MDL RDL Notes QC1200185MB1 Di-n-butyl phthalate 93 J ug/Kg 67 250 Di-n-octyl phthalate ND ug/Kg 23 250 Fluoranthene ND ug/Kg 21 250 Fluorene ND ug/Kg 27 250 - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - Hexachlorobenzene ND ug/Kg 15 250 Hexachlorobutadiene ND ug/Kg 39 250 Hexachlorocyclopentadiene ND ug/Kg 14 1200 Hexachloroethane ND ug/Kg 43 250 - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - Indeno(1,2,3-cd)pyrene ND ug/Kg 90 250 Isophorone ND ug/Kg 25 250 Naphthalene ND ug/Kg 25 250 Nitrobenzene ND ug/Kg 21 1200 - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - N-Nitrosodimethylamine(NDMA) ND ug/Kg 34 250 N-Nitrosodi-n-propylamine(NDPA) ND ug/Kg 26 250 N-Nitrosodiphenylamine ND ug/Kg 24 250 Pentachlorophenol ND ug/Kg 55 1200 - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - Phenanthrene ND ug/Kg 22 250 Phenol ND ug/Kg 26 250 Pyrene ND ug/Kg 23 250 Pyridine ND ug/Kg 21 250 - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - Total Cresol ND ug/Kg 400 400 Lab Control Spike/Lab Control Spike Duplicate Summary Spike Amount Spike Result Recoveries Limits Analyte LCS LCSD LCS LCSD Units LCS LCSD RPD %Rec RPD Notes QC1200185LCS1 1,2,4-Trichlorobenzene 2000 1400 ug/Kg 70 43-111 1,4-Dichlorobenzene 2000 1300 ug/Kg 65 30-116 2,4,5-Trichlorophenol 2000 1600 ug/Kg 80 57-125 2,4-Dimethylphenol 2000 1300 ug/Kg 65 50-112 - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 2,4-Dinitrotoluene 2000 1500 ug/Kg 75 57-124 2-Chlorophenol 2000 1200 ug/Kg 60 48-114 3 and 4-Methylphenol(m and p-Cresol) 2000 1500 ug/Kg 75 56-124 4-Chloro-3-m ethyl phenol 2000 1500 ug/Kg 75 61-122 - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 4-Nitrophenol 2000 1500 ug/Kg 75 54-126 Acenaphthene 2000 1300 ug/Kg 65 53-112 Benzo(b)fluoranthene 2000 1500 ug/Kg 75 61-125 Chrysene 2000 1500 ug/Kg 75 59-117 - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - N-Nitrosodi-n-propylamine(NDPA) 2000 1400 ug/Kg 70 54-110 Pentachlorophenol 2000 1200 ug/Kg 60 41-103 Phenol 2000 1300 ug/Kg 65 51-111 Pyrene 2000 1600 ug/Kg 80 63-119 Matrix Spike/Matrix Spike Duplicate Summary Sample Spike Amount Spike Result Recoveries Limits Analyte Amount MS MSD MS MSD Units MS MSD RPD %Rec RPD Notes QC1200185MS1,QC1200185MSD1 Source: 413666-003 1,2,4-Trichlorobenzene ND 2000 2000 1100 850 ug/Kg 55 43 25.6 35-93 30 1,4-Dichlorobenzene ND 2000 2000 940 690 ug/Kg 47 35 30.7 39-95 30 M 2,4,5-Trichlorophenol ND 2000 2000 1400 1200 ug/Kg 70 60 15.4 44-108 30 2,4-Dimethylphenol ND 2000 2000 1200 940 ug/Kg 60 47 24.3 37-105 30 2,4-Dinitrotoluene ND 2000 2000 2000 1900 ug/Kg 100 95 5.1 48-109 30 2-Chlorophenol ND 2000 2000 980 730 ug/Kg 49 37 29.2 42-102 30 M Analytical Results Report Enthalpy 98808-01 Lab Request 413685,Page 8 of 14 Analytical,LLC