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QCBatchlD: QC1200211 Analyst: dswafford Method: EPA 6010B Matrix: Solid Analyzed: 03/26/2019 Instrument: AAICP(group) Blank Summary Blank Analyte Result Units MDL RDL Notes QC 1200211 M B 1 Antimony 1.52 J mg/Kg 0.37 3 Arsenic 0.56 J mg/Kg 0.36 1 Barium ND mg/Kg 0.23 1 Beryllium ND mg/Kg 0.17 0.5 Cadmium ND mg/Kg 0.21 0.5 Chromium ND mg/Kg 0.13 1 Cobalt ND mg/Kg 0.19 0.5 Copper ND mg/Kg 0.31 1 - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - Lead 0.79 J mg/Kg 0.32 1 Molybdenum 0.20 J mg/Kg 0.13 1 Nickel ND mg/Kg 0.2 1.5 Selenium ND mg/Kg 0.72 3 Silver ND mg/Kg 0.13 0.5 Thallium 1.23 J mg/Kg 0.42 3 Vanadium ND mg/Kg 0.37 0.5 Zinc 1.82 J mg/Kg 0.28 5 - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -- Lab Control Spike/Lab Control Spike Duplicate Summary Spike Amount Spike Result Recoveries Limits Analyte LCS LCSD LCS LCSD Units LCS LCSD RPD %Rec RPD Notes OC1200211LCS1 Antimony 100 99.1 mg/Kg 99 80-120 Arsenic 100 105 mg/Kg 105 80-120 Barium 100 100 mg/Kg 100 80-120 Beryllium 100 107 mg/Kg 107 80-120 Cadmium 100 102 mg/Kg 102 80-120 Chromium 100 97.1 mg/Kg 97 80-120 Cobalt 100 103 mg/Kg 103 80-120 Copper 100 99.8 mg/Kg 100 80-120 Lead 100 107 mg/Kg 107 80-120 Molybdenum 100 105 mg/Kg 105 80-120 Nickel 100 106 mg/Kg 106 80-120 Selenium 100 97.3 mg/Kg 97 80-120 - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - Silver 100 100 mg/Kg 100 80-120 Thallium 100 95.0 mg/Kg 95 80-120 Vanadium 100 100 mg/Kg 100 80-120 Zinc 100 109 mg/Kg 109 80-120 Matrix Spike/Matrix Spike Duplicate Summary Sample Spike Amount Spike Result Recoveries Limits Analyte Amount MS MSD MS MSD Units MS MSD RPD %Rec RPD Notes QC1200211MS1,QC1200211MSD1 Source: 413710-001 Antimony 2.32 100 100 44.8 57.4 mg/Kg 42 55 24.7 75-125 20 M,D Arsenic 2.98 100 100 97.6 97.9 mg/Kg 95 95 0.3 75-125 20 Barium 79.2 100 100 176 162 mg/Kg 97 83 8.3 75-125 20 Beryllium ND 100 100 98.8 94.9 mg/Kg 99 95 4.0 75-125 20 - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - Cadmium 0.56 100 100 90.3 89.4 mg/Kg 90 89 1.0 75-125 20 Chromium 11.5 100 100 99.8 97.7 mg/Kg 88 86 2.1 75-125 20 Cobalt 6.28 100 100 94.7 95.7 mg/Kg 88 89 1.1 75-125 20 Copper 9.72 100 100 98.2 98.1 mg/Kg 88 88 0.1 75-125 20 Lead 8.84 100 100 101 103 mg/Kg 92 94 2.0 75-125 20 Molybdenum 0.31 100 100 88.1 93.0 mg/Kg 88 93 5.4 75-125 20 Analytical Results Report Enthalpy 98808-01 Lab Request 413685, Page 10 of 14 Analytical,LLC