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GeoAnalytical Laboratories, Inc. <br />2300 Maryann Dr. Turlock, CA 95380 Phone (209) 669-0100 Fax(209)593-2212 <br />email: info@geoanalyticallab.com <br />Report # E8L1709 Project: American Tire and Truck Repair Date: 02/07/19 <br />San Joaquin County Environmental Health Date Rec'd: 12/17/18 <br />1868 East Hazelton Ave <br />Stockton, CA 95205 <br />Inorganic Chemistry - Quality Control <br />GeoAnalytical Laboratories, Inc. <br />Reporting Spike Source %REC RPD <br />Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br />Batch F000406 - 3010A Prepared: 02/06/19 Analyzed: 02/07/19 <br />Matrix Spike (F000406 -MSI) <br />Source: E8LI709-01 <br />Antimony <br />0.011 <br />0.010 mg/L <br />0.006250 <br />0.004 <br />117 <br />80-120 <br />Arsenic <br />0.028 <br />0.010 <br />0.01250 <br />0.015 <br />100 <br />80-120 <br />Barium <br />0.250 <br />0.100 <br />0.02500 <br />0.275 <br />NR <br />80-120 <br />QM -4X <br />Beryllium <br />0.006 <br />0.010 <br />0.006250 <br />ND <br />104 <br />80-120 <br />Cadmium <br />0.013 <br />0.001 <br />0.01250 <br />0.001 <br />98 <br />80-120 <br />Chromium <br />0.028 <br />0.010 <br />0.02500 <br />0.005 <br />95 <br />80-120 <br />Cobalt <br />0.022 <br />0.010 <br />0.02500 <br />ND <br />89 <br />80-120 <br />Copper <br />0.043 <br />0.010 <br />0.02500 <br />0.022 <br />85 <br />80-120 <br />Molybdenum <br />0.043 <br />0.005 <br />0.006250 <br />0.038 <br />88 <br />80-120 <br />Nickel <br />0.028 <br />0.050 <br />0.02500 <br />ND <br />113 <br />80-120 <br />Selenium <br />0.014 <br />0.010 <br />0.01250 <br />ND <br />110 <br />80-120 <br />Silver <br />0.011 <br />0.020 <br />0.01250 <br />ND <br />89 <br />80-120 <br />Thallium <br />0.006 <br />0.010 <br />0.006250 <br />ND <br />94 <br />80-120 <br />Vanadium <br />0.019 <br />0.010 <br />0.01250 <br />0.006 <br />97 <br />80-120 <br />Zinc <br />0.219 <br />0.050 <br />0.02500 <br />0.193 <br />105 <br />80-120 <br />QM -4X <br />Mercury <br />0.0013 <br />0.001 <br />0.001250 <br />ND <br />104 <br />80-120 <br />Matrix Spike Dup (F000406-MSDI) <br />Source: E8L1709-01 <br />Antimony <br />0.011 <br />0.010 mg/L <br />0.006250 <br />0.004 <br />124 <br />80-120 <br />4 <br />20 <br />QM -07 <br />Arsenic <br />0.028 <br />0.010 <br />0.01250 <br />0.015 <br />103 <br />80-120 <br />1 <br />20 <br />Barium <br />0.268 <br />0.100 <br />0.02500 <br />0.275 <br />NR <br />80-120 <br />7 <br />20 <br />QM -4X <br />Beryllium <br />0.007 <br />0.010 <br />0.006250 <br />ND <br />105 <br />80-120 <br />1 <br />20 <br />Cadmium <br />0.013 <br />0.001 <br />0.01250 <br />0.001 <br />99 <br />80-120 <br />1 <br />20 <br />Chromium <br />0.029 <br />0.010 <br />0.02500 <br />0.005 <br />97 <br />80-120 <br />2 <br />20 <br />Cobalt <br />0.023 <br />0.010 <br />0.02500 <br />ND <br />91 <br />80-120 <br />2 <br />20 <br />Copper <br />0.044 <br />0.010 <br />0.02500 <br />0.022 <br />90 <br />80-120 <br />3 <br />20 <br />Molybdenum <br />0.045 <br />0.005 <br />0.006250 <br />0.038 <br />112 <br />80-120 <br />3 <br />20 <br />Nickel <br />0.029 <br />0.050 <br />0.02500 <br />ND <br />114 <br />80-120 <br />1 <br />20 <br />Selenium <br />0.014 <br />0.010 <br />0.01250 <br />ND <br />114 <br />80-120 <br />3 <br />20 <br />Silver <br />0.011 <br />0.020 <br />0.01250 <br />ND <br />88 <br />80-120 <br />0.7 <br />20 <br />Thallium <br />0.006 <br />0.010 <br />0.006250 <br />ND <br />98 <br />80-120 <br />4 <br />20 <br />Vanadium <br />0.019 <br />0.010 <br />0.01250 <br />0.006 <br />99 <br />80-120 <br />1 <br />20 <br />-Zinc <br />0.223 <br />0.050 <br />0.02500 <br />0.193 <br />122 <br />80-120 <br />2 <br />20 <br />QM -4X <br />Mercury <br />0.0013 <br />0.001 <br />0.001250 <br />ND <br />105 <br />80-120 <br />0.8 <br />20 <br />Certification # 2585 <br />