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Q�C [ C�Q�uOo I�"Il Lt <br /> Analytical Laboratory CERTIFICATE OFAIVALYSIS <br /> Friday,April 4, 2008 <br /> Attention: Guy W.Roy <br /> R&L Diesel <br /> P.O.Box 2498 Report Page 33 of4l <br /> Danville, CA 94526 <br /> fu.v. <br /> I <br /> Volatile Organic Compounds bbl EPA Method 8260B <br /> Sample In}brmatibn <br /> Sample ID: B3 -29 Sample Type: Grab <br /> <` Laboratory ID: 8030609-07 Project Name: UST-Waste Oil <br /> Date/Time Sampled.• 06-Mar-08 14:15 by Guy W.Roy Sample Matrix: Soil <br /> �.3 <br /> a Test Parameter Result DLR '1 Unit Dilution Batch Prepared Ana sis Date Method Notes <br /> Trichloroethene ND 2.00 ;uglkg 1 AC81102 11-Mar-08 11-Mar-O8 EPA 8260E <br /> (s <br /> Trichlorofluoromethane ND 2.00 iugltcg 1 AC81102 11-Mar-08 11-Mar-O8 EPA 8260E <br /> 1,2,3-Trichloropropane ND 2.00 :ug/kg 1 AC81102 11-Mar-08 11-Mar-08 EPA 8260B <br /> w; <br /> 1,3,5 Trimethylbenzene 46.0 2.00 uglkg 1 AC81102 11-Mar-08 11-Mar-08 EPA 8260B <br /> 1,2,4-Trimethylbenzene 159 2.00 ug/kg 1 AC61102 11-Mar-08 11-Mar-08 EPA 82608 <br /> 4 <br /> Vinyl acetate <br /> Y ND 20.0 ug/kg 1 AC61102 11-Mar-0B 11-Mar-08 EPA 82606 <br /> Vinyl chloride'Y Y ND 2.00 ug/kg 1 AC81102 11-Mar-0B 11-Mar-08 EPA 82608 <br /> Methyl tert-butyl Ether(MtSE) ND 2.00 ug/kg 1 AC81102 11-Mar-08 11-Mar-08 EPA 8260E <br /> n m,p-Xylene 12.5 2.00 ug/kg 1 AC61102 11-Mar-08 1 i-Mar-08 EPA$2606 <br /> Ethyl tent-Butyl e=ther(ETBE) ND 2.00 ug/kg 1 AC61102 11-Mar-08 11-Mar-08 EPA 826013 <br />' <br /> Xylene o-X <br /> Y 13.8 2_00 ug/kg 1 AC91102 11-Mar-OS 11-Mar-0B EPA 82608 <br /> ' tert-Amyl Methyl Ether(TAME) ND 2.00 ug/kg 1 AC61102 11-Mar-08 11-Mar-08 EPA 8260B <br /> tert-Butyl Acohol(TBA) ND 50.0 ug/kg 1 AC61102 11-Mar-08 11-Mar-O8 EPA 82606 <br /> Diisopropyl Ether(RIPE) ND 2.00 ug/kg 1 AC6,1102 11-Mar-08 11-Mar-08 EPA 82608 <br /> Surrogate:Dibromofluoromethane 109% 86-118 <br /> Surrogate:Toluene-d8 88% 88-110 <br /> Surrogate:4-Bromofluorobenzene 88% 86-115 <br /> y <br />� L <br /> t I <br />.E <br /> 1 <br /> S <br /> mg/L=milligrams per Liter=ppm DLR—Detection Limit for Purpose of Reporting. <br /> ug/L=micrograms per Liter—ppb Exceptional sample matrices or interferences may <br /> result in higher detection limits. <br /> RESPECTFULLY SUBMITTED, <br /> (��/Ow�- <br /> Jonathan Lc,Laboratory Director <br /> 3935 N. Coronado Ave. Stockton, CA 95204 Tel.: 209) 477-8105 Fax: (209) 546-7497 <br /> - � ti <br />