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,ItaN �� 2018 <br /> CASTLE ANALYTICAL LABORATORY <br /> Environmental Testing Services 2333 Shuttle Drive,Atwater,CA 95301 P#jone: (209)384-2930 <br /> Certificate#2480 E=fir,t t( [)V_ ix.� r (�'� Fax: (209)384-1507 <br /> ACT Environmental Services Client Project Name:Value Products Method:EPA 5030/8260B <br /> 265 Riggs Ave. Lab Reference Number:1901020 Instrument ID:VARIAN MS <br /> Merced, CA 95341 Sample Description:Water Prepared: 01-15-19 <br /> Attn:Jose Moran Analyzed: 01-15-19 <br /> Reported: 01-17-19 <br /> QUALITY CONTROL DATA REPORT <br /> SPIKE ID: VWMS-1159 <br /> Reporting BLANK Spiking Control %R <br /> Limit Result Level Spike Limits <br /> u /L u /L u /L %R <br /> COMPOUNDS <br /> t-But I Alcohol(t-BA) 10 ND 75 96.3% 70-130% <br /> Methyl t-but I ether (MTBE) 0.50 ND 2.5 130% 70-130% <br /> Diiso ro I ether DIPS 0.50 ND 2.5 126% 70-130% <br /> Ethyl t-But I ether ETBE 0.50 ND 2.5 82.4% 70-130% <br /> t-Am I methyl ether TAME 0.50 ND 2.5 93.6% 70-130% <br /> 1,2-Dichloroethane 1,2-DCA 0.50 ND 2.5 100% 70-130% <br /> Ethylene dibromide EDB 0.50 ND 2.5 118% 70-130% <br /> 1,1-Dichloroethene 1,1,DCE 0.50 ND 2.5 132% 70-130% <br /> Benzene 0.50 ND 2.5 124% 70-130% <br /> Trichloroethene(TCE) 0.50 ND 2.5 130% 70-130% <br /> Toluene 0.50 ND 2.5 118% 70-130% <br /> Chlorobenzene 0.50 ND 2.5 112% 70-130% <br /> Surro ate: <br /> Dibromofluoromethane 1.0 113% 10 114% 70-130% <br /> 1,2-Dichloroethane-d4 1.0 110% 10 1 97.7% 70-130% <br /> Toluene-d8 1.0 95.9% 10 1 108% 70-130% <br /> 4-Bromofluorobenzene 1.0 107% 10 108% 70-130% <br /> Spiking MATRIX MATRIX %R %RPD <br /> Level SPIKE SPIKE DUP Limits <br /> u IL %R %R <br /> COMPOUNDS <br /> t-But I Alcohol t-BA 75 99.9% 89.0% 70-130% 10.4% <br /> Methyl t-butyl ether MTBE 2.5 118% 96.8% 70-130% 20.1% <br /> Diiso ro I ether DIPE 2.5 124% 124% 70-130% 0.323% <br /> Ethyl t-But I ether ETBE 2.5 110% 92.8% 70-130% 17.3% <br /> t-Am I methyl ether TAME 2.5 108% 90.8% 70-130% 15.7% <br /> 1,2-Dichloroethane 1,2-DCA 2.5 106% 94.0% 70-130% 11.6% <br /> Ethylene dibromide EDB 2.5 126% 105% 70-130% 18.0% <br /> 1,1-Dichloroethene(1,1,DCE) 2.5 126% 114% 70-130% 9.00% <br /> Benzene 2.5 119% 100% 70-130% 15.1% <br /> Trichloroethene(TCE) 2.5 127% 106% 70-130% 17.9% <br /> Toluene 2.5 164% 107% 70-130% 38.9% <br /> Chlorobenzene 2.5 104% 96.8% 70-130% 7.17% <br /> Surrogate: <br /> Dibromofluoromethane 10 117% 107% 70-130% 8.99% <br /> 1,2-Dichloroethane-d4 10 107% 97.1% 70-130% 9.33% <br /> Toluene-d8 10 101% 92.7% 70-130% 8.57% <br /> 4-Bromofluorobenzene 10 99.0% 105% 70-130% 6.26% <br /> APPROVED BY: <br /> James C.PRIX-PS/La oratory Director or <br /> Clan J. Cone/L boratory Manager <br />