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Laboratory Control Spike Recovery METALS APPL Inc. 4203 West Swift Avenue Fresno, CA 93722 Method Compound Name Spike Level SPK Result SPK% Recovery Extract Analysis mg/kg mg/kg Recovery Limits Date Date QC Group EPA 6010B Antimony(Sb) 25 25.4 102 75-125 10/14/2004 0/15/2004 $CAMS-041014A-AP76743 EPA 6010B Arsenic(As) 25 25.5 102 75-125 10/14/2004 0/15/2004 $CAMS-041014A-AP76743 EPA 6010B Barium (Ba) 25 26.2 105 75-125 10/14/2004 0/15/2004 $CAMS-041014A-AP76743 EPA 6010B Beryllium (Be) 5 5.0 100 75-125 10/14/2004 0/15/2004 $CAMS-041014A-AP76743 EPA 6010B Cadmium (Cd) 5 5.3 106 75-125 10/14/2004 0/15/2004 $CAMS-041014A-AP76743 EPA 6010B Chromium (Cr) 25 26.2 105 75-125 10/14/2004 0/15/2004 $CAMS-041014A-AP76743 EPA 6010B Cobalt(Co) 25 26.3 105 75-125 10/14/2004 0/15/2004 $CAMS-041014A-AP76743 EPA 6010B Copper(Cu) 25 25.7 103 75-125 10/14/2004 0/15/2004 $CAMS-041014A-AP76743 c EPA 6010B Lead (Pb) 25 26.5 106 75-125 10/14/2004 0/15/2004 $CAMS-041014A-AP76743 EPA 6010B Molybdenum (Mo) 25 27.0 108 75-125 10/14/2004 0/15/2004 $CAMS-041014A-AP76743 EPA 6010B Nickel (Ni) 25 26.4 106 75-125 10/14/2004 0/15/2004 $CAMS-041014A-AP76743 EPA 6010B Selenium (Se) 25 24.4 97.6 75-125 10/14/2004 0/15/2004 $CAMS-041014A-AP76743 EPA 6010B Silver(Ag) 10 9.9 99.0 75-125 10/14/2004 0/15/2004 $CAMS-041014A-AP76743 EPA 6010B Thallium (TI) 25 26.6 106 75-125 10/14/2004 0/15/2004 $CAMS-041014A-AP76743 EPA 6010B Vanadium (V) 25 26.8 107 75-125 10/14/2004 0/15/2004 $CAMS-041014A-AP76743 EPA 6010B Zinc(Zn) 50 53.8 108 75-125 10/14/2004 0/15/2004 $CAMS-041014A-AP76743 EPA 7471A Mercury 0.667 0.67 100 80-120 10/14/2004 0/15/2004 $HG-S-041014A-AP76743 Comments: Printed: 10/20/2004 11:09:32 AM APPL Standard LCS