COMPLIANCE INFO_1993 - 1994 - Laserfiche WebLink

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STANDARD PROVISIONS AND REPORTING REQUIREMENTS September 1993 FOR WASTE DISCHARGE REQUIREMENTS FOR DISCHARGES REGULATED BY CHAPTER 15 AN"D/OR PART 258 _8- must conform to EPA guidelines (e.g., "Laboratory Documentation Requirements for Data Validation," January 1990, USEPA Region 9) or to procedures approved by the Board. j. The director of the laboratory whose name appears on the certification shall supervise all analytical work in his/her laboratory and shall sign all reports of such work submitted to the Regional Board. 6. Unless samples are from water supply wells or unless otherwise specified by the Executive Officer, all ground water samples to be analyzed for metals shall be field-filtered. Filtration methods shall minimize the entrainment of air into the sample (by using, for example. in-line pressure filtration). Sampling and Analytical Methods For any given monitored medium, the samples taken from all Monitoring Points and Background Monitoring Points to satisfy the data analysis requirements for a given Reporting Period shall all be taken within a span not exceeding 30 days, unless the Executive Officer approves a longer time period, and shall be taken in a manner that ensures sample independence to the greatest extent feasible. 2. Specific methods of collection and analysis must be identified. Sample collection, storage, and analysis shall be performed according to the most recent version of USEPA Methods, such as the latest editions, as applicable, of: (1) "Methods for Organic Chemical Analysis of Municipal and Industrial Wastewater" (EPA 600 Series), (2) "Test Methods for Evaluating Solid Waste" (SW 846-latest edition), and (3) "Methods for Chemical Analysis of Water and Wastes," and in accordance with an approved sampling and analysis plan. If methods other than USEPA-approved methods or Standard Methods are used, the exact methodology must be submitted for review and must be approved by the Executive Officer prior to use. 3. The methods of analysis and the detection limits used must be appropriate for the expected concentrations. For detection monitoring of any constituent or parameter that is found in concentrations which produce more than 90% non-numerical determinations (i.e., "trace" or "ND") in data from Background Monitoring Points for that medium, the analytical method having the lowest method detection limit (MDL) shall be selected from among those methods which would provide valid results in light of any matrix effects or interferences. 4. "Trace"results—results falling between the MDL and the practical quantitation limit (PQL)— shall be reported as such, and shall be accompanied both by the estimated MDL and PQL values for that analytical run.