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Oilfield Environmental and Compliance, INC. <br /> CalRecycle Project: PG5 <br /> 1001 I Street Project Number: 2512 Vineyard Ave Reported: <br /> Sacramento CA,95814 Project Manager: Glenn Young 10-May-13 14:39 <br /> Volatile Organic Compounds by EPA Method TO-15-Quality Control <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch A304732-EPA TO-15 prep <br /> LCS(A304732-BSI) Prepared&Analyzed:27-Apr-13 <br /> Ethyl t-Butyl Ether 10.0 0.50 ppbv 10.0 100 0-200 <br /> Methylene chloride 9.80 0.50 10.0 98.0 29-190 <br /> Methyl-t-butyl ether 10.1 0.50 10.0 101 58-145 <br /> Styrene 10.4 0.50 10.0 104 61-141 <br /> t-Amyl Methyl Ether 10.3 0.50 10.0 103 0-200 <br /> t-Butyl alcohol 9.41 0.50 10.0 94.1 0-200 <br /> Tetrachloroethene(PCE) 9.56 0.50 10.0 95.6 61-131 <br /> Toluene 8.03 0.50 10.0 80.3 60-131 <br /> 1,1,1-Trichloroethane 10.3 0.50 10.0 103 59-140 <br /> Trichloroethene(TCE) 9.73 0.50 10.0 97.3 66-131 <br /> Trichlorofluoromethane 9.94 0.50 10.0 99.4 52-155 <br /> Vinyl chloride 10.4 0.50 10.0 104 26-197 <br /> Xylenes(total) 27.6 0.50 30.0 92.2 60-139 <br /> Duplicate(A304732-DUPI) Source: 1301753-15 Prepared:27-Apr-13 Analyzed:28-Apr-13 <br /> Acetone ND 10 ppbv ND 25 <br /> Benzene ND 10 ND 25 <br /> Benzyl chloride ND 10 ND 25 <br /> Bromodichloromethane ND 10 ND 25 <br /> Bromoform ND 10 ND 25 <br /> Bromomethane ND 40 ND 25 <br /> 1,3-Butadiene ND 10 ND 25 <br /> Carbon disulfide ND 10 ND 25 <br /> Carbon tetrachloride ND 10 ND 25 <br /> Chlorobenzene ND 10 ND 25 <br /> Chloroethane ND 10 ND 25 <br /> Chloroform ND 10 ND 25 <br /> Chloromethane ND 20 ND 25 <br /> Cyclohexane ND 10 ND 25 <br /> Dibromochloromethane ND 10 ND 25 <br /> 1,2-Dibromoethane(EDB) ND 10 ND 25 <br /> 1,2-Dichlorobenzene ND 10 ND 25 <br /> 1,3-Dichlorobenzene ND 10 ND 25 <br /> 1,4-Dichlorobenzene 11.2 10 10.6 5.50 25 <br /> Dichlorodifluoromethane ND 10 ND 25 <br /> 1,1-Dichloroethane ND 10 ND 25 <br /> 1,2-Dichloroethane ND 10 ND 25 <br /> 1,1-Dichloroethene ND 10 ND 25 <br /> cis-1,2-Dichloroethene ND 10 ND 25 <br /> trans-1,2-Dichloroethene ND 10 ND 25 <br /> 1,2-Dichloropropane ND 10 ND 25 <br /> Oilfield Environmental and Compliance The results in this report apply to the samples analyred in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> TEL: (805) 922-4772 <br /> 307 Roemer Way, Suite 300, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 <br /> Page 50 of 72 <br />