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Oilfield Environmental and Compliance, INC. <br /> CalRecycle Project: PG5 <br /> 1001 I Street Project Number: 2512 Vineyard Ave Reported: <br /> Sacramento CA,95814 Project Manager: Glenn Young 10-May-13 14:39 <br /> Volatile Organic Compounds by EPA Method TO-15-Quality Control <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch A304741 -EPA TO-15 prep <br /> LCS(A304741-BS1) Prepared&Analyzed:29-Apr-13 <br /> Ethyl t-Butyl Ether 9.40 0.50 ppbv 10.0 94.0 0-200 <br /> Methylene chloride 9.28 0.50 10.0 92.8 29-190 <br /> Methyl-t-butyl ether 9.49 0.50 10.0 94.9 58-145 <br /> Styrene 9.83 0.50 10.0 98.3 61-141 <br /> t-Amyl Methyl Ether 9.38 0.50 10.0 93.8 0-200 <br /> t-Butyl alcohol 9.10 0.50 10.0 91.0 0-200 <br /> Tetrachloroethene(PCE) 9.19 0.50 10.0 91.9 61-131 <br /> Toluene 7.65 0.50 10.0 76.5 60-131 <br /> 1,1,1-Trichloroethane 9.58 0.50 10.0 95.8 59-140 <br /> Trichloroethene(TCE) 9.35 0.50 10.0 93.5 66-131 <br /> Trichlorofluoromethane 9.65 0.50 10.0 96.5 52-155 <br /> Vinyl chloride 10.2 0.50 10.0 102 26-197 <br /> Xylenes(total) 26.2 0.50 30.0 87.3 60-139 <br /> LCS Dup(A304741-BSDI) Prepared&Analyzed:29-Apr-13 <br /> Benzene 11.4 0.50 ppbv 10.0 114 63-130 21.2 25 <br /> Bromomethane 12.2 2.0 10.0 122 12-233 22.9 25 <br /> Carbon tetrachloride 12.2 0.50 10.0 122 61-130 21.7 25 <br /> Chlorobenzene 11.7 0.50 10.0 117 69-123 22.0 25 <br /> Chloroform 11.5 0.50 10.0 115 56-144 22.6 25 <br /> 1,2-Dibromoethane(EDB) 11.9 0.50 10.0 119 58-141 21.2 25 <br /> 1,3-Dichlorobenzene 11.8 0.50 10.0 118 34-182 22.3 25 <br /> 1,4-Dichlorobenzene 11.6 0.50 10.0 116 46-175 16.6 25 <br /> Dichlorodifluoromethane 11.9 0.50 10.0 119 53-168 21.7 25 <br /> 1,2-Dichloroethane 12.0 0.50 10.0 120 57-154 22.0 25 <br /> 1,1-Dichloroethene 11.5 0.50 10.0 115 43-163 22.6 25 <br /> 1,2-Dichloropropane 11.9 0.50 10.0 119 61-130 22.0 25 <br /> Diisopropyl Ether 11.3 0.50 10.0 113 0-200 20.6 25 <br /> Ethanol 12.0 0.50 10.0 120 28-177 23.6 25 <br /> Ethylbenzene 10.3 0.50 10.0 103 53-139 21.1 25 <br /> Ethyl t-Butyl Ether 11.7 0.50 10.0 117 0-200 21.7 25 <br /> Methylene chloride 11.7 0.50 10.0 117 29-190 23.1 25 <br /> Methyl-t-butyl ether 11.8 0.50 10.0 118 58-145 21.7 25 <br /> Styrene 12.4 0.50 10.0 124 61-141 23.0 25 <br /> t-Amyl Methyl Ether 12.0 0.50 10.0 120 0-200 24.8 25 <br /> t-Butyl alcohol 11.4 0.50 10.0 114 0-200 22.3 25 <br /> Tetrachloroethene(PCE) 11.5 0.50 10.0 115 61-131 22.2 25 <br /> Toluene 9.53 0.50 10.0 95.3 60-131 21.9 25 <br /> 1,1,1-Trichloroethane 12.0 0.50 10.0 120 59-140 22.3 25 <br /> Trichloroethene(TCE) 11.5 0.50 10.0 115 66-131 20.5 25 <br /> Trichlorofluoromethane 11.9 0.50 10.0 119 52-155 20.8 25 <br /> Oilfield Environmental and Compliance The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> TEL: (805) 922-4772 <br /> 307 Roemer Way, Suite 300, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 <br /> Page 54 of 72 <br />