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Oilfield Environmental and Compliance, INC. <br /> CalRecycle Project:Lodi City Landfill <br /> 432 Geranium Circle Project Number: Turner Drive,Lodi Reported: <br /> Galt,CA 95632 CA,95814 Project Manager: Sabra Ambrose 16-May-12 15:29 <br /> Volatile Organic Compounds by EPA Method TO-15-Quality Control <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch A205212-EPA TO-15 prep <br /> LCS(A205212-BS1) Prepared&Analyzed:09-May-12 <br /> Benzene 5.50 0.50 ppbv 5.00 110 67-133 <br /> Bromomethane 4.58 2.0 5.00 91.6 13-226 <br /> Carbon tetrachloride 4.76 0.50 5.00 95.2 70-141 <br /> Chlorobenzene 5.43 0.50 5.00 109 73-132 <br /> Chloroform 4.58 0.50 5.00 91.6 36-192 <br /> 1,2-Dibromoethane(EDB) 5.21 0.50 5.00 104 33-200 <br /> 1,3-Dichlorobenzene 6.17 0.50 5.00 123 70-139 <br /> 1,4-Dichlorobenzene 5.99 0.50 5.00 120 70-143 <br /> Dichlorodifluoromethane 4.98 0.50 5.00 99.6 52-157 <br /> 1,2-Dichloroethane 5.26 0.50 5.00 105 55-152 <br /> 1,1-Dichloroethene 4.23 0.50 5.00 84.6 61-133 <br /> 1,2-Dichloropropane 5.46 0.50 5.00 109 62-142 <br /> Ethanol 3.80 0.50 5.00 76.0 45-144 <br /> Ethylbenzene 5.45 0.50 5.00 109 59-142 <br /> Methylene chloride 4.80 0.50 5.00 96.0 57-158 <br /> Methyl-t-butyl ether 4.47 0.50 5.00 89.4 77-136 <br /> Styrene 5.37 0.50 5.00 107 67-165 <br /> Tetrachloroethene(PCE) 5.39 0.50 5.00 108 70-130 <br /> Toluene 5.83 0.50 5.00 117 65-141 <br /> 1,1,1-Trichloroethane 4.81 0.50 5.00 96.2 72-133 <br /> Trichloroethene(TCE) 5.38 0.50 5.00 108 68-128 <br /> Trichlorofluoromethane 4.30 0.50 5.00 86.0 69-139 <br /> Vinyl chloride 4.51 0.50 5.00 90.2 59-139 <br /> Xylenes(total) 15.5 0.50 15.0 103 74-140 <br /> Surrogate:Dibromofluoromethane 22 25.0 88.4 0-249 <br /> Surrogate:Toluene-d8 28 25.0 111 53-164 <br /> Surrogate:4-Bromofluoroberr_ene 28 25.0 113 60-146 <br /> Oilfield Environmental and Compliance The results in this report apply to the samples analy_ed in accordance with the chain of <br /> custody document. This analytical report must be reproduced in its entirety. <br /> TEL: (805) 922-4772 <br /> 307 Roemer Way, Suite 300, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 <br /> Page 33 of 36 <br />