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Oilfield Environmental and Compliance, INC. <br /> CalRecycle Project: Lodi City Landfill <br /> 432 Geranium Circle Project Number: Awani Drive Reported: <br /> Galt,CA 95632 CA,95814 Project Manager: Sabra Ambrose 09-Jul-12 12:30 <br /> Volatile Organic Compounds by EPA Method TO-15-Quality Control <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch A207013-EPA TO-15 prep <br /> LCS(A207013-BS2) Prepared&Analyzed:02-Jul-12 <br /> Diisopropyl Ether 6.33 0.50 ppbv 5.00 127 0-200 CCFH <br /> Ethyl t-Butyl Ether 6.14 0.50 5.00 123 0-200 <br /> t-Amyl Methyl Ether 5.82 0.50 5.00 116 0-200 <br /> t-Butyl alcohol 4.76 0.50 5.00 95.2 0-200 <br /> Surrogate:Dibromo luoromethane 24 25.0 95.3 0-198 <br /> Surrogate:Toluene-d8 26 25.0 102 63-135 <br /> Surrogate:4-Bromo luorobensene 12 25.0 49.4 56-155 S-GC <br /> LCS Dup(A207013-BSDI) Prepared&Analyzed:02-Jul-12 <br /> Benzene 4.76 0.50 ppbv 4.78 99.6 62-133 1.91 25 <br /> Bromomethane 6.76 2.0 4.29 158 26-189 23.4 25 CCFH <br /> Carbon tetrachloride 4.75 0.50 4.92 96.4 55-135 0.00 25 <br /> Chlorobenzene 4.60 0.50 4.96 92.7 68-128 1.75 25 <br /> Chloroform 5.91 0.50 4.90 121 54-137 1.53 25 <br /> 1,2-Dibromoethane(EDB) 5.15 0.50 4.96 104 51-149 0.194 25 <br /> 1,3-Dichlorobenzene 4.77 0.50 5.65 84.4 34-192 0.631 25 <br /> 1,4-Dichlorobenzene 4.86 0.50 5.10 95.3 43-185 0.619 25 <br /> Dichlorodifluoromethane 6.53 0.50 4.85 135 53-155 3.76 25 CCFH <br /> 1,2-Dichloroethane 6.25 0.50 4.91 127 56-150 1.94 25 <br /> 13-Dichloroethene 5.81 0.50 4.68 124 42-150 1.20 25 <br /> 1,2-Dichloropropane 4.94 0.50 4.86 102 57-131 2.25 25 <br /> Ethanol 4.65 0.50 4.08 114 27-164 26.0 25 QR-02 <br /> Ethylbenzene 4.33 0.50 5.15 84.1 61-138 2.06 25 <br /> Methylene chloride 6.26 0.50 5.25 119 38-164 0.637 25 <br /> Methyl-t-butyl ether 5.87 0.50 4.92 119 57-138 2.94 25 <br /> Styrene 4.46 0.50 5.30 84.2 65-144 1.81 25 <br /> Tetrachloroethene(PCE) 5.08 0.50 4.91 103 56-136 0.592 25 <br /> Toluene 4.58 0.50 5.00 91.7 56-137 1.98 25 <br /> 1,1,1-Trichloroethane 5.73 0.50 4.93 116 57-134 0.350 25 <br /> Trichloroethene(TCE) 5.34 0.50 4.84 110 62-130 3.24 25 <br /> Trichlorofluoromethane 5.89 0.50 4.85 121 52-143 0.508 25 <br /> Vinyl chloride 5.17 0.50 4.79 108 24-188 27.2 25 CCFH, <br /> QR-02 <br /> Xylenes(total) 13.0 0.50 15.7 82.5 68-137 1.15 25 <br /> Surrogate:Dibromo luoromethane 23 25.0 92.7 0-198 <br /> Surrogate:Toluene-d8 25 25.0 101 63-135 <br /> Surrogate:4-Bromo luoroben_ene 24 25.0 95.4 56-155 <br /> Oilfield Environmental and Compliance The results in this report apply to the samples analysed in accordance with the chain of <br /> custody document. This analytical report must be reproduced in its entirety. <br /> TEL: (805) 922-4772 <br /> 307 Roemer Way, Suite 300, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 <br /> Page 30 of 33 <br />