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Sequoia <br />Analytical <br />E <br />U <br />819 Striker Avenue, Suite 8 <br />Sacramento, CA 95834 <br />(916) 921-9600 <br />FAX (916) 921-0100 <br />KleinWder - Stockton <br />Client Project ID: <br />20-3978-01.W36 <br />5amplecl: <br />Jun <br />1(, <br />1999 <br />2825 East Myrtle St. <br />Sample Descript: <br />Soil, 18964-CS4 <br />Received: <br />Jun <br />22, <br />1999 <br />Stockton, CA 95205 <br />Analysis Method: <br />EPA 3550/8270 <br />Extracted: <br />Jun <br />25, <br />1999 <br />Attention: Tony Martin <br />Lab Number: <br />S906400 -04 <br />Analyzed: <br />Jun <br />29, <br />1999 <br />..................................... <br />N.D. <br />N.D. <br />Reported: <br />Jul <br />13, <br />1999 <br />IAnalyte <br />Reporting Limit <br />Ng/kg <br />Sample Results <br />Ng/kg <br />Analytes reported as N.D. were not detected at or above the reporting limit. <br />SEQUOIA ANALYTICAL, FLAP #1271 <br />Sandra R. Hanson 1 <br />Project Manager/Sacramento Laboratory Page 2 of 2 <br />S906400.KLF <10> <br />1 <br />Di-n-octyl phthalate........................................................... <br />Fluoranthene.................................................................... <br />250 <br />250 <br />..................................... <br />N.D. <br />N.D. <br />Fluorene........................................................................... <br />250 <br />..................................... <br />N.D. <br />Hexachlorobenzene......................................................... <br />Hexachlorobutadiene....................................................... <br />250 <br />250 <br />N.D. <br />N.D. <br />Hexachlorocyclopentadiene............................................. <br />Hexachloroethane............................................................ <br />500 <br />250 <br />..................................... <br />..................................... <br />N.D. <br />N.D. <br />Indeno(1,2,3-cd)pyrene.................................................... <br />Isophorone........................................................................ <br />2-Methylnaphthalene........................................................ <br />2-Methylphenol................................................................. <br />4-Methylphenol................................................................. <br />Naphthalene..................................................................... <br />2-Nitroaniline.................................................................... <br />250 <br />250 <br />250 <br />250 <br />250 <br />250 <br />500 <br />..................................... <br />..................................... <br />..................................... <br />..................................... <br />..................................... <br />..................................... <br />N.D. <br />N.D. <br />N.D. <br />N.D. <br />N.D. <br />N.D. <br />N.D. <br />3-NitroaniIine.................................................................... <br />4-Nitroaniline.................................................................... <br />500 <br />500 <br />..................................... <br />N.D. <br />N.D. <br />Nitrobenzene.................................................................... <br />250 <br />..................................... <br />N. D. <br />2-Nitrophenol.................................................................... <br />4-Nitrophenol.................................................................... <br />N-Nitrosodiphenylamine................................................... <br />N-Nitroso-di-n-propylamine.............................................. <br />Pentachlorophenol............................................................ <br />Phenanthrene................................................................... <br />250 <br />500 <br />250 <br />250 <br />500 <br />250 <br />..................................... <br />..................................... <br />..................................... <br />..................................... <br />..................................... <br />N.D. <br />N.D. <br />N.D. <br />N.D. <br />N.D. <br />N.D. <br />Phenol.............................................................................. <br />250 <br />..................................... <br />N.D. <br />Pyrene.............................................................................. <br />1,2',4-Trichlorobenzene. . <br />2,4,5-Trichlorophenol........................................................ <br />2,4,6-Trichlorophenol........................................................ <br />250 <br />250 <br />500 <br />250 <br />..................................... <br />..................................... <br />N.D. <br />N. D. <br />N.D. <br />N.D. <br />Surrogates <br />2-Fluorophenol................................................. <br />Phenol-d6......................................................................... <br />Control Limits, % <br />25-121 <br />24-113 <br />..................................... <br />..................................... <br />% Recovery <br />63 <br />63 <br />Nitrobenzene-d5............................................................... <br />23-120 <br />..................................... <br />73 <br />2-Fluorobiphenyl............................................................... <br />2,4, 6-Tribromophenol....................................................... <br />4-Terphenyl-d 14............................................................... <br />30-115 <br />19-122 <br />18-137 <br />..................................... <br />..................................... <br />70 <br />75 <br />73 <br />Analytes reported as N.D. were not detected at or above the reporting limit. <br />SEQUOIA ANALYTICAL, FLAP #1271 <br />Sandra R. Hanson 1 <br />Project Manager/Sacramento Laboratory Page 2 of 2 <br />S906400.KLF <10> <br />1 <br />