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SEMI -VOLATILE ORGANICS by GC/S (EPA 8270) <br />= Analyte Reporting Limit Sample Results <br />N9/kg Ng/kg <br />Di-n-octyl phthalate........................................................... <br />Fluoranthene.................................................................... <br />250 <br />250 <br />..................................... <br />is <br />Sequoia <br />Fluorene........................................................................... <br />819 Striker Avenue, Suite 8 <br />Sacramento, CA 95834. <br />is <br />N.D. <br />(916) 921-9600 <br />FAX (916) 921 -0100 <br />-AnalytSam <br />>'Klen�eTder.''Stockto <br />1 <br />N.D. <br />N.D. <br />P le <br />*2825 East Myrtle St. <br />Sample Descript: <br />Method Blank <br />Received: N/A <br />Stockton, CA 95205 <br />Analysis Method: <br />EPA 3550/8270 <br />Extracted: Jun 25, 1999 <br />:Attention: Ton Martin <br />Tony <br />Lab Number: <br />BLK062599 <br />Analyzed: Jun 28, 1999 <br />N.D. <br />N.D. <br />Reported: Jul 13, 1999 <br />SEMI -VOLATILE ORGANICS by GC/S (EPA 8270) <br />= Analyte Reporting Limit Sample Results <br />N9/kg Ng/kg <br />Surrogates <br />2-Fluorophenol................................................................ <br />Phenol-d6....................................................................... <br />Nitrobenzene -d5 ............................................................. <br />2-Fluorobiphenyl............................................................. <br />2,4,6-Tribromophenol..................................................... <br />4-Terphenyl-d 14............................................................. <br />Control Limits, % <br />25-121 <br />24-113 <br />23-120 <br />30-115 <br />19-122 <br />18-137 <br />Analytes reported as N.D. were not detected at or above the reporting limit. <br />SEQUOIA ANALYTICAL, ELAP #1271 <br />Sandra R. Hanson <br />Project Manager/Sacramento Laboratory Page 2 of 2 <br />% Recovery <br />63 <br />61 <br />72 <br />71 <br />69 <br />67 <br />S906400.KLF <12> <br />1 <br />Di-n-octyl phthalate........................................................... <br />Fluoranthene.................................................................... <br />250 <br />250 <br />..................................... <br />N.D. <br />N.D. <br />Fluorene........................................................................... <br />250 <br />..................................... <br />N.D. <br />Hexachlorobenzene......................................................... <br />Hexachlorobutadiene....................................................... <br />250 <br />250 <br />N.D. <br />N.D. <br />Hexachlorocyclopentadiene............................................. <br />Hexachloroethane............................................................ <br />500 <br />250 <br />..................................... <br />..................................... <br />N.D. <br />N.D. <br />Indeno(1,2,3-cd)Pyrene.................................................... <br />Isophorone........................................................................ <br />2-Methylnaphthalene........................................................ <br />2-MethyIpheno1................................................................. <br />4-Methylphenol................................................................. <br />Naphthalene..................................................................... <br />2-Nitroaniline.................................................................... <br />250 <br />250 <br />250 <br />250 <br />250 <br />250 <br />500 <br />..................................... <br />..................................... <br />..................................... <br />..................................... <br />......... I........................... <br />N.D. <br />N.D. <br />N.D. <br />N.D. <br />N.D. <br />N.D. <br />N.D. <br />3-Nitroaniline.................................................................... <br />4-Nitroaniline.................................................................... <br />500 <br />500 <br />N.D. <br />N.D. <br />Nitrobenzene.................................................................... <br />250 <br />..................................... <br />N.D. <br />2-Nitrophenol.................................................................... <br />4-Nitrophenol.................................................................... <br />N-Nitrosodiphenylamine................................................... <br />N-Nitroso-di-n-propylamine.............................................. <br />Pentachlorophenol............................................................ <br />Phenanthrene................................................................... <br />250 <br />500 <br />250 <br />250 <br />500 <br />250 <br />..................................... <br />..................................... <br />................... <br />..................................... <br />..................................... <br />N.D. <br />N.D. <br />N.D. <br />N.D. <br />N.D. <br />N.D. <br />Phenol.............................................................................. <br />250 <br />..................................... <br />N.D. <br />Pyrene.............................................................................. <br />1,2,4-Trichlorobenzene.................................................... <br />2,4,5-Trichlorophenol........................................................ <br />2,4,6-Trichlorophenol........................................................ <br />250 <br />250 <br />500 <br />250 <br />..................................... <br />......... <br />..................................... <br />N.D. <br />N.D. <br />N.D. <br />N.D. <br />Surrogates <br />2-Fluorophenol................................................................ <br />Phenol-d6....................................................................... <br />Nitrobenzene -d5 ............................................................. <br />2-Fluorobiphenyl............................................................. <br />2,4,6-Tribromophenol..................................................... <br />4-Terphenyl-d 14............................................................. <br />Control Limits, % <br />25-121 <br />24-113 <br />23-120 <br />30-115 <br />19-122 <br />18-137 <br />Analytes reported as N.D. were not detected at or above the reporting limit. <br />SEQUOIA ANALYTICAL, ELAP #1271 <br />Sandra R. Hanson <br />Project Manager/Sacramento Laboratory Page 2 of 2 <br />% Recovery <br />63 <br />61 <br />72 <br />71 <br />69 <br />67 <br />S906400.KLF <12> <br />1 <br />