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* No head space over sample. ** This is the maximum holding time prior to extraction. The extracted sample may be held r up to 40 days before anvlysis. *** RCRA holding time is 7 days. Note: All solid samples should be collected in stainless steel sleeves, brass sleeves or in glass jars all with teflon -lined caps and 4-8 oz. capacity. All solid samples should be kept cool at 4 C. ' Section No: 6 Page: 14 of 16 Revision No: 2.0 Date: January 15, 1994 Sampling Procedures TAB 6-1 RECOMMENDEDS LE COLLECTION AND PRESERVATION Volume Holding A 1 si,a f&uLaLncr LMU Preservation Time Organic Chemicals W&qewater and =rdous Waste 1" A 601/8010* G, VOA 2 x 40 Na S20 , if chlorinated 14 days TFE-septa cap HLI, p2 < 2; Cool, 4 C EPA 8011 G, VOA 2 x 40 Na2S2033, if chlorinated 28 days TFE-septa cap Cool, 4 C EPA 602/8020* G, VOA 2 x 40 Na S20 , if chlorinated 14 days TFE-septa cap , p <2; Cool, 4 C EPA 603/8030* G, VOA TFE-septa 2 x 40 Na S20 , if chlorinated AcOu.4 -H to 4-5; Cool, 4 C 14 days J cap P EPA 604/8040** G, amber 1 x 1000 Na2S203, if chlorinated 7 days TFE-lined cap Cool, 4 C EPA 608/8080** G, amber 1 x 1000 Na2S2033, if chlorinated 7 days TFE-lined cap Cool, 4 C , EPA 610/8310 G, amber 1 x 1000 Na020 , if chlorinated 14 days TFE-Iined cap Cool, 4 EPA 613** G, amber 1 x 1000 Na2S20 , if chlorinated 7 days -lined cap Cool, 4 EPA 614/8140** G, amber 1 x 1000 Cool, 4 C 7 days TFE-lined cap ` t EPA 615/8150** G, amber i x 1000 Na2S20 , if chlorinated 7 days TFE-lined cap Cool, 4 EPA 619 G, amber 1 x 1000 Na02033, if chlorinated 14 days TFF,-Iined cap Cool, 4 C * No head space over sample. ** This is the maximum holding time prior to extraction. The extracted sample may be held r up to 40 days before anvlysis. *** RCRA holding time is 7 days. Note: All solid samples should be collected in stainless steel sleeves, brass sleeves or in glass jars all with teflon -lined caps and 4-8 oz. capacity. All solid samples should be kept cool at 4 C.