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OW " <br />Section No: 9 <br />Page: 12 of 13 <br />Revision No: 2.0 <br />Date: January 15, 1994 <br />Analytical Procedures -1 <br />TABLE 9-3 Specific Analytical Solid Waste / Hazardous Waste Methods <br />Parameter Method DescriptiOT <br />pH EPA 9045 ISE <br />Phosphorous <br />Phosphate (PO4) EPA 9056 IC <br />Total (P) See Tram Metals <br />Sulfate (SO4) EPA 9056 IC <br />Sulfide (H2S) EPA 376.2 Colorimetric <br />Hazardous Waste Characterization Analyses <br />Corrosivity (pH) <br />Aqueous sample <br />EPA 9040 <br />ISE <br />Nonaqueous sample <br />EPA 9045 <br />ISE <br />Ignitability <br />EPA 1310 <br />Extraction <br />Aqueous (Flashpoint) <br />EPA 1010 <br />Flashpoint <br />Nonaqueous (Flammability) <br />EPA 1020 <br />Flashpoint <br />Reactivity <br />SW4146 Ch 8 <br />Observations <br />Reaction with water <br />EPA 7041 <br />Furnace Atomic Absorption <br />Reaction with dilate acid <br />EPA 6020 <br />ICP,/MS <br />Reaction with dilute base <br />EPA 7060 <br />Furnace Atomic Absorption <br />Reaction with oxidizing agent <br />EPA 6020 <br />ICP/MS <br />Reaction with reducing agent <br />EPA 6010 <br />ICP <br />Generation <br />SW4146 Ch 7 <br />Sareens; <br />Sulfide <br />EPA 6010 <br />ICP <br />Cyanide <br />EPA 6020 <br />ICP/MS <br />Sample Preparation - TTLC <br />EPA 3050 <br />Digestion <br />Sample Preparation - S <br />Title 22 <br />Extraction <br />Sample Preparation - EP TOX <br />EPA 1310 <br />Extraction <br />Sample Preparation - TC LP <br />EPA 1311 <br />Extraction <br />Aluminum (Al) <br />EPA 6010 <br />ICP <br />Aluminum (Al) <br />EPA 6020 <br />ICP/MS <br />Antimony (Sb) <br />EPA 7041 <br />Furnace Atomic Absorption <br />Antimony (Sb) <br />EPA 6020 <br />ICP,/MS <br />Arsenic (As) <br />EPA 7060 <br />Furnace Atomic Absorption <br />Arsenic (As) <br />EPA 6020 <br />ICP/MS <br />Barium (Ba) <br />EPA 6010 <br />ICP <br />Barium (Ba) <br />EPA 6020 <br />ICP/MS <br />Beryllium (Be) <br />EPA 6010 <br />ICP <br />Beryllium (Be) <br />EPA 6020 <br />ICP/MS <br />Boron (B) <br />EPA 6010 <br />ICP <br />Boron (B) <br />EPA 6020 <br />ICP/MS <br />Cadmium (Cd) <br />EPA 6010 <br />ICP <br />Cadmium (Cd) <br />EPA 6020 <br />ICP,/MS <br />Calcium (Ca) <br />EPA 6010 <br />ICP <br />Chromium (Cr) <br />EPA 6010 <br />ICP <br />Chromium (Cr) <br />EPA 6010 <br />ICP/MS <br />Chromium VI (Cr+6) <br />EPA 7196 <br />Colorimetric <br />