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819 Striker Ave Ste 8 <br /> Sequoia Sacramento,CA 95834 <br /> (916)921-9600 <br /> Analytical FAXequoi labs.c00 <br /> 1 wwwsequoialabs.com <br /> Shaw E&I-Sacramento Project: Corral Hollow Landfill,San Joaquin County S310191 <br /> 1326 N.Market Blvd. Project Number: 791291/00004000 Reported: <br /> Sacramento CA,95834 Project Manager: Steve Giacomini 12/04/03 14:58 <br /> Conventional Chemistry Parameters by APHA/EPA Methods-Quality Control <br /> ' Sequoia Analytical-Petaluma <br /> Reporting Spike Source %REC RPD <br /> Analyte Result MDL Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch 3100309-General Preparation <br /> Blank(3100309-BLKI) Prepared:10/13/03 Analyzed: 10/14/03 <br /> ' Total Organic Carbon ND 0.048 0.20 mg/I <br /> Laboratory Control Sample(3100309-BSI) Prepared: 10/13/03 Analyzed: 10/14/03 <br /> Total Organic Carbon 9.01 0.048 0.20 mg/l 10.0 90 80-120 <br /> Matrix Spike(3100309-MS1) Source:P310169-01 Prepared:10/13/03 Analyzed: 10/14/03 <br /> Total Organic Carbon 9.32 0.097 0.40 mg/I 10.0 0.30 90 75-125 <br /> Matrix Spike Dup(3100309-MSD1) Source:P310169-01 Prepared: 10/13/03 Analyzed: 10/14/03 <br /> Total Organic Carbon 9.28 0.097 0.40 mg/l 10.0 0.30 90 75-125 0.4 20 <br /> Batch 3100325-General Preparation <br /> Blank(3100325-BLK1) Prepared 9, A-1-1- 10/14/03 <br /> Sulfide ND 7.0 25 mg/1 <br /> Laboratory Control Sample(3100325-BS1) Prepared&Analyzed: 10/14/03 <br /> Sulfide 112 7.0 25 mg/I 114 98 80-120 <br /> Laboratory Control Sample Dup(3100325-BSDI) Prepared&Analyzed:10/14/03 <br /> Sulfide 116 7.0 25 mg/l 114 102 80-120 4 20 <br /> Batch 3100548-General Preparation <br /> Blank(3100548-BLKI) Prepared&Analyzed: 10/22/03 <br /> Cyanide(total) ND 0.0050 0.0050 mg/1 <br /> The results in this report apply to the samples analyzed in accordance with the chain of <br /> Sequoia Analytical-Sacramento � PPY P Y <br /> custody document.Unless otherwise stated,results are reported on a wet weight basis. <br /> ' This analytical report must be reproduced in its entirety. <br /> Page 40 of 66 <br />