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819 Striker Ave Ste 8 <br /> Sequoia Sacramento,CA 95834 <br /> (916)921-9600 <br /> -0 100 <br /> Analytical FAXequoi92 s.com <br /> wwwsequoialabs.com <br /> _ Project: Corral Hollow Landfill,San Joaquin County S310191 <br /> Shaw E&I Sacramento 1 9 tY <br /> 1326 N.Market Blvd. Project Number. 791291/00004000 Reported: <br /> Sacramento CA,95834 Project Manager. Steve Giacomini 12/04/03 14:58 <br /> Volatile Organic Compounds by EPA Method 8260B - Quality Control <br /> ' Sequoia Analytical-Sacramento <br /> Reporting Spike Source %REC RPD <br /> Analyte Result MDL Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch 3100255-EPA 5030B [P/TI <br /> Blank(3100255-BLK1) Prepared&Analyzed: 10/17/03 <br /> ' Methyl tert-butyl ether ND 0.36 0.50 ug/1 <br /> Naphthalene ND 0.93 1.0 <br /> n Propylbenzene ND 0.37 0.50 <br /> Styrene ND 0.33 0.50 " <br /> ' 1,1,1,2-Tetrachloroethane ND 0.34 0.50 <br /> 1,1,2,2-Tetrachloroethane ND 0.59 1.0 <br /> Tetrachloroethene ND 0.44 0.50 " <br /> Toluene ND 0.32 0.50 " <br /> 1,2,3-Trichlorobenzene ND 0.46 0.50 " <br /> 1,2,4-Trichlorobenzene ND 0.41 0.50 " <br /> 1,1,1-Trichloroethane ND 0.19 0.50 " <br /> 1,1,2-Trichloroethane ND 0.43 0.50 " <br /> Trichloroethene ND 0.36 0.50 <br /> Trichlorofluoromethane ND 0.42 0.50 " <br /> 1,2,3-Trichloropropane ND 0.55 1.0 " <br /> 1,2,4-Trimethylbenzene ND 0.18 0.50 <br /> 1,3,5-Trimethylbenzene ND 028 0.50 <br /> Vinyl chloride ND 0.16 0.50 " <br /> ' Xylenes(total) ND 0.48 0.50 ~ <br /> Surrogate:Dibromofluoromethane 24.9 25.0 100 70-130 <br /> Surrogate:l,2-DCA-d4 16.1 25.0 104 70-130 <br /> Surrogate:Toluene-d8 15.1 25.0 100 70-130 <br /> ' <br /> Surrogate:4-BFB 25.7 25.0 103 70-130 <br /> Blank(3100255-BLK2) Prepared&Analyzed: 10/21/03 <br /> 2-Bulanone ND 0.14 0.50 ug/1 <br /> ' 2-Chloroethylvinyl ether ND 022 0.50 p <br /> 2-Hexanone ND 026 0.50 <br /> 4-Methyl-2-pentanone ND 0.17 0.50 " <br /> Acetone 1.05 0.52 2.0 J <br /> ' Acetonitrile ND 2.4 5.0 " <br /> Acrolein ND 0.70 5.0 <br /> Acrylonitrile ND 0.26 2.0 " <br /> Allyl chloride ND 0.14 0.50 „ <br /> Carbon disulfide ND 0.29 0.50 <br /> Chloroprene ND 0.10 0.50 " <br /> ' cis-1,3-Dichloropropene ND 0.11 0.50 " <br /> Sequoia Analytical-Sacramento The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.Unless otherwise stated,results are reported on a wet weight basis. <br /> This analytical report must be reproduced in its entirety. <br /> Page 53 of 66 <br />