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819 Striker Ave Ste 8 <br /> Sequoia Sacram(916 )921to,CA95834 <br /> -9600 <br /> Analytical FAXequoi labs.c00 <br /> www.sequoialabs.com <br /> Shaw E&I-Sacramento Project: Corral Hollow Landfill,San Joaquin County S310191 <br /> 1326 N.Market Blvd. Project Number: 791291/00004000 Reported: <br /> Sacramento CA,95834 Project Manager: Steve Giacomini 12/04/03 14:58 <br /> Volatile Organic Compounds by EPA Method 8260B- Quality Control <br /> Sequoia Analytical-Sacramento <br /> Reporting Spike Source %REC RPD <br /> Analyte Result DtDL Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch 3100255-EPA 5030B [P/T] <br /> Laboratory Control Sample(3100255-BS3) Prepared&Analyzed: 10/22/03 <br /> Benzene 24.9 0.28 0.50 ug/l 25.0 100 70-130 <br /> Chl6robenzene 25.4 0.32 0.50 25.0 102 70-130 <br /> 1,1-Dichloroethene 25.1 024 0.50 25.0 100 70-130 <br /> Toluene 26.0 0.32 0.50 25.0 104 70-130 <br /> Trichloroethene 19.2 0.36 0.50 25.0 77 70-130 <br /> Surrogate:Dibromo luoromethane 24.1 25.0 96 70-130 <br /> Surrogate:1,2-DCA-d4 15.0 25.0 100 70-130 <br /> Surrogate:Toluene-d8 15.2 25.0 101 70-130 <br /> Surrogate:4-BFB 15.4 25.0 102 70-130 <br /> Matrix Spike(3100255 MSI) Source:S310191-04 Prepared&Analyzed: 10/21/03 <br /> Benzene 24.5 0.28 0.50 ug/l 25.0 ND 98 60-140 <br /> Chlorobenzene 25.3 0.32 0.50 25.0 ND 101 60-140 <br /> 1,1-Dichloroethene 21.5 024 0.50 25.0 ND 86 60-140 <br /> Toluene 26.2 0.32 0.50 25.0 1.0 101 60-140 <br /> Trichloroethene 18.2 0.36 0.50 25.0 ND 73 60-140 <br /> Surrogate:DibromoJluoromethane 23.9 25.0 96 70-130 <br /> Surrogate:1,2-DCA-d4 24.7 25.0 99 70-130 <br /> ' Surrogate:Toluene-d8 15.2 25.0 101 70-130 <br /> Surrogate:4-BFB 25.4 25.0 102 70-130 <br /> Matrix Spike Dup(3100255 MSD1) Source:5310191-04 Prepared&Analyzed: 10/21/03 <br /> Benzene 23.3 028 0.50 ug/l 25.0 ND 93 60-140 5 25 <br /> ' Chlorobenzene 24.8 032 0.50 11 25.0 ND 99 60-140 2 25 <br /> 1,1-Dichloroethene 20.5 024 0.50 25.0 ND 82 60-140 5 25 <br /> Toluene 26.1 032 0.50 25.0 1.0 100 60-140 0.4 25 <br /> Trichloroethene 17.3 0.36 0.50 II 25.0 ND 69 60-140 5 25 <br /> Surrogate:DibromoJluoromethane 24.2 25.0 97 70-130 <br /> Surrogate:1,2-DCA-d4 25.1 25.0 100 70-130 <br /> Surrogate:Toluene-d8 25.8 25.0 103 70-130 <br /> Surrogate:4-BFB 25.9 25.0 104 70-130 <br /> Sequoia Analytical-Sacramento <br /> The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document. Unless otherwise stated,results are reported on a wet weight basis. <br /> This analytical report must be reproduced in its entirety. <br /> Page 59 of 66 <br />