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.NVM) 819 Striker Ave Ste 8 <br /> Sequoia Sacramento,CA 95834 <br /> (916)921-9600 <br /> at t FAX(916)921-0100 <br /> Analytical a l www.sequoialabs.com <br /> Shaw E&I-Sacramento Project: Corral Hollow Landfill,San Joaquin County S310191 <br /> 1326 N.Market Blvd. Project Number: 791291/00004000 Reported: <br /> Sacramento CA,95834 Project Manager: Steve Giacomini 12/04/03 14:58 <br /> Anions by EPA Method 300.0 -Quality Control <br /> Sequoia Analytical-Sacramento <br /> Reporting Spike Source %REC RPD <br /> Analyte Result MDL Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch 3100216-General Preparation <br /> Blank(3100216-BLK1) Prepared&Analyzed: 10/09/03 <br /> Chloride ND 0.031 0.20 mg/1 <br /> Nitrate as N ND 0.0045 0.023 <br /> Sulfate as SO4 ND 0.031 0.20 <br /> Laboratory Control Sample(3100216-BSI) Prepared&Analyzed: 10/09/03 <br /> Chloride 4.80 0.031 0.20 mg/I 5.00 96 80-120 <br /> Nitrate as N 1.12 0.0045 0.023 1.13 99 80-120 <br /> Sulfate as SO4 10.1 0.031 0.20 10.0 101 80-120 <br /> Laboratory Control Sample Dup(3100216-BSD1) Prepared&Analyzed: 10/09/03 <br /> Chloride 4.78 0.031 0.20 mg/1 5.00 96 80-120 0.4 200 <br /> Nitrate as N 1.12 0.0045 0.023 1.13 99 80-120 0 200 <br /> Sulfate as SO4 10.1 0.031 0.20 10.0 101 80-120 0 200 <br /> Matrix Spike(3100216-MS1) Source:5310220-05 Prepared&Analyzed: 10/09/03 <br /> Chloride 61.1 0.031 0.20 mg/l 5.00 59 42 75-125 QM-07 <br /> Nitrate as N 11.2 0.0045 0.023 " 1.13 9.4 159 75-125 QM-07 <br /> Sulfate as SO4 23.4 0.031 0.20 10.0 15 84 75-125 <br /> Matrix Spike(3100216-MS2) Source:S310197-01 Prepared&Analyzed: 10/09/03 <br /> Chloride 48.7 0.31 2.0 mg/l 50.0 ND 97 75-125 <br /> Nitrate as N 11.5 0.045 0.23 " 11.3 0.13 101 75-125 <br /> Sulfate as SO4 102 0.31 2.0 100 ND 102 75-125 <br /> Sequoia Analytical-Sacramento The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.Unless otherwise stated,results are reported on a wet weight basis. <br /> This analytical report must be reproduced in its entirety. <br /> Page 65 of 66 <br />