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819 Striker Ave Ste 8 <br /> Sequoia Sacramento,CA 95834 <br /> 1 (916)921.9600 <br /> FAXAnalytical www.sequoialabs.com <br /> Shaw E&1-Sacramento Project Corral Hollow Landfill,San Joaquin County S308356 <br /> 1326 N.Market Blvd. Project Number. 791291/00003000 Reported: <br /> Sacramento CA,95834 Project Manager. Steve Giacomini 09/03/03 16:39 <br /> Volatile Organic Compounds by EPA Method 8260B-Quality Control <br /> Sequoia Analytical-Sacramento <br /> Reporting Spike Source °.LREC RPD <br /> Malyte Result MDL Limit Units Level Result %REC Limits RPD Limit Notes <br /> _Batch 3080311-EPA 5030B[P/T] <br /> Blank(3080311-BLKI) Prepared&Analyzed:0822/03 <br /> 2-Butanone ND 0.14 0.50 ug/i <br /> 2-Chloroethylvinyl ether ND 0.22 0.50 " <br /> 2-Hexanone ND 0.26 0.50 n <br /> 4-Methyl-2-pentanone ND 0.17 0.50 <br /> Acetone 1.80 0.52 2.0 J <br /> Acetonitrile ND 2.4 5.0 " <br /> Acrolein ND 0.70 5.0 " <br /> Acrylonitrile ND 0.26 2.0 " <br /> Allyl chlori& ND 0.14 0.50 " <br /> Carbon disulfide ND 0.29 0.50 " <br /> Chloroprene ND 0.10 0.50 <br /> cis-1,3-Dichloropropene ND 0.I1 0.50 " <br /> Freon 113 ND 0.25 0.50 " <br /> Iodomethane ND 0.036 0.50 <br /> Isobutanol ND 0.61 1.0 <br /> m,p-Xylene ND 0.38 0.50 <br /> Methacrylonitrile ND 0.73 1.0 " <br /> Methyl methacrylate ND 0.20 0.50 <br /> o-Xylene ND 0.15 0.50 <br /> Propionitrile ND 2.7 5.0 <br /> trans-1,3-Dichloropropene ND 0.10 0.50 " <br /> trans-1,4-Dichloro-2-butane ND 0.42 0.50 w <br /> Vinyl acetate ND 0.94 2.0 <br /> Benzene ND 0.28 0.50 <br /> Bromobenzene ND 0.39 0.50 " <br /> Bromochloromethane ND 0.42 0.50 N <br /> Bromodichloromethane ND 0.25 0.50 <br /> Bromoform ND 0.18 0.50 " <br /> Bromomethane 0.700 0.61 1.0 l <br /> n-Butylbenzene ND 0.38 0.50 <br /> sec-Butylbenzene ND 0.36 0.50 <br /> tert Butylbenzene ND 0.35 0.50 <br /> Carbon tetrachloride ND 0.37 0.50 a <br /> Chlorobenzene ND 0.32 0.50 <br /> Chloroethane ND 0.31 0.50 <br /> Chloroform ND 0.37 0.50 " <br /> Chloromethane 0.230 0.18 0.50 J <br /> Sequoia Analytical-Sacramento The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.Unless otherwise stated,results are reported on a wet weight basis. <br /> This analytical report must be reproduced in its entirety. <br /> Page 11 of 17 <br />