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r919 Striker Ave Ste 8 <br /> Sequoia Sacramento.CA 95834 <br /> (916)921.9600 <br /> Analytical FAX(916)921-0100 <br /> www.sequoialabs.com <br /> Shaw E&I-Sacramento Project: Corral Hollow Landfill,San Joaquin County 5308356 <br /> 1326 N.Market Blvd. Project Number. 791291/00003000 Reported: <br /> Sacramento CA,95834 Project Manager: Steve Giacomini 09/03/03 16:39 <br /> Volatile Organic Compounds by EPA Method 8260B-QuaIity Control <br /> Sequoia Analytical-Sacramento <br /> Reporting Spike Source %REC RPD <br /> Analyte Result MDL Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch 3080311-EPA 5030B[P/T] <br /> Blank(3080311-BLKI) Prepared&Analyzed:08/22/03 <br /> Trichlorofluoromethane ND 0.42 0.50 ug/I <br /> 1,2,3-Trichloropropane ND 0.55 1.0 " <br /> 1,2,4-Trimethylbenzene ND 0.18 0.50 K <br /> 1,3,5-Trimethylbenzene ND 0.28 0.50 <br /> Vinyl chloride ND 0.16 0.50 <br /> Xylenes(total) ND 0.48 0.50 " <br /> Surrogate:Dibromofluoromethane 25.0 25.0 100 70-130 <br /> Surrogate:1,2-DCA-d4 25.9 25.0 104 70-130 <br /> Surrogate:Toluene-d8 24.4 25.0 98 70-130 <br /> Surrogate:4-BFB 26.8 25.0 107 70-130 <br /> Laboratory Control Sample(3080311-BSI) Prepared&Analyzed:08/22/03 <br /> ® Benzene 24.7 0.28 0.50 ug/I 25.0 99 70-130 <br /> Chlorobenzene 24.0 0.32 0.50 25.0 96 70-130 <br /> 1,1-Dichloroethene 23.2 0.24 0.50 n 25.0 93 70-130 <br /> Toluene 23.8 0.32 0.50 25.0 95 70-130 <br /> Trichloroethene 21.3 0.36 0.50 25.0 85 70-130 <br /> Surrogate:Dibromofluoromethane 26.3 25.0 105 70-130 <br /> Surrogate:1,2-DCA-d4 25.7 I, 25.0 103 70-130 <br /> Surrogate:Toluene-d8 23.6 25.0 94 70-130 <br /> Surrogate:4-BFB 26.3 " 25.0 105 70-130 <br /> ' Matrix Spike(3080311-MS1) Source:S308418-01 Prepared:08/22/03 Analyzed:08/23/03 <br /> Benzene 25.2 0.28 0.50 ug/l 25.0 13 96 60-140 <br /> Chlorobenzene 24.0 0.32 0.50 25.0 ND 96 60-140 <br /> I,1-Dichloroethene 32.1 0.24 0.50 " 25.0 ND 128 60-140 <br /> Toluene 24.2 0.32 0.50 25.0 0.44 95 60-140 <br /> Trichloroethene 22.3 0.36 0.50 25.0 ND 89 60-140 <br /> Surrogate:Dibromofluoromethane 17.8 25.0 111 70-130 <br /> Surrogate:1,2-DCA-d4 28.6 25.0 114 70-130 <br /> Surrogate:Toluene-d8 24.1 25.0 96 70-130 <br /> Surrogate:4-BFB 27.0 25.0 108 70-130 <br /> Sequoia Analytical-Sacramento The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.Unless otherwise stated results are reported on a wet weight basis. <br /> This analytical report must be reproduced in its entirety. <br /> Page 13 of 17 <br />